Microwave-assisted synthesis of mono- And disubstituted 4-hydroxyacetophenone derivatives via Mannich reaction: Synthesis, XRD and HS-analysis
An efficient microwave-assisted one-step synthetic route toward Mannich bases is developed from 4-hydroxyacetophenone and different secondary amines in quantitative yields, via a regioselective substitution reaction. The reaction takes a short time and is
Synthesis and Insecticidal Activity of Some New 3-Substituted 4-Hydroxyacetophenones
A number of 3-(N,N-dialkylaminomethyl)-4-hydroxy acetophenones (4-10) and their thiophosphorylated compounds (11-16) have been synthesised and screened for their insecticidal activity.Only thiophosphorylated compounds are found to possess significant activity.The intramolecular hydrogen bonding in these compounds has also been discussed.
Borthakur, R. C.,Borthakur, N.,Rastogi, R. C.
p. 244 - 248
(2007/10/02)
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