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1092563-20-6

1092563-20-6

Identification

  • Product Name:N-(4-(2-cyanoacetyl)-5-oxo-5,6-dihydro-4H-1,3,4-thiadiazin-2-yl)benzamide

  • CAS Number: 1092563-20-6

  • EINECS:

  • Molecular Weight:302.313

  • Molecular Formula: C13H10N4O3S

  • HS Code:

  • Mol File:1092563-20-6.mol

Synonyms:N-(4-(2-cyanoacetyl)-5-oxo-5,6-dihydro-4H-1,3,4-thiadiazin-2-yl)benzamide

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Relevant articles and documentsAll total 1 Articles be found

Heterocyclic synthesis with 4-benzoyl-1-cyanoacetylthiosemicarbazide: Selective synthesis of some thiazole, triazole, thiadiazine, pyrrylthiazole, and pyrazolo[1,5-a]triazine derivatives

Bondock, Samir,El-Gaber Tarhoni, Abd,Fadda, Ahmed A.

, p. 153 - 159 (2008)

4-Benzoyl-1-cyanoacetylthiosemicarbazide undergoes coupling reaction with aromatic diazonium chloride to afford (arylhydrazono)thiosemicarbazide, which was reacted with phenacyl bromide regioselectivity to afford the thiazoline. The (arylhydrazono)thiosem

Process route upstream and downstream products

Process route

cyanoacetic acid 2'-[(benzoylamino)thiocarbonyl]hydrazide
54779-96-3

cyanoacetic acid 2'-[(benzoylamino)thiocarbonyl]hydrazide

ethyl bromoacetate
105-36-2

ethyl bromoacetate

N-(4-(2-cyanoacetyl)-5-oxo-5,6-dihydro-4H-1,3,4-thiadiazin-2-yl)benzamide
1092563-20-6

N-(4-(2-cyanoacetyl)-5-oxo-5,6-dihydro-4H-1,3,4-thiadiazin-2-yl)benzamide

Conditions
Conditions Yield
With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 20h;
61%
cyanoacetic acid 2'-[(benzoylamino)thiocarbonyl]hydrazide
54779-96-3

cyanoacetic acid 2'-[(benzoylamino)thiocarbonyl]hydrazide

ethyl bromoacetate
105-36-2

ethyl bromoacetate

N-(4-(2-cyanoacetyl)-5-oxo-5,6-dihydro-4H-1,3,4-thiadiazin-2-yl)benzamide
1092563-20-6

N-(4-(2-cyanoacetyl)-5-oxo-5,6-dihydro-4H-1,3,4-thiadiazin-2-yl)benzamide

Conditions
Conditions Yield
With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 20h;
61%

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