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Cas Database

125023-41-8

125023-41-8

Identification

  • Product Name:N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide

  • CAS Number: 125023-41-8

  • EINECS:

  • Molecular Weight:299.37

  • Molecular Formula: C18H21NO3

  • HS Code:

  • Mol File:125023-41-8.mol

Synonyms:N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide

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Relevant articles and documentsAll total 1 Articles be found

A directed metalation of N-tert-butyl-N-methyl-2-methoxybenzamide. Short syntheses of 2-methoxy-6-methylbenzoic acid and lunularic acid

Reitz,Massey

, p. 1375 - 1379 (1990)

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Process route upstream and downstream products

Process route

2-Methoxybenzoyl chloride
21615-34-9

2-Methoxybenzoyl chloride

N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide
125023-41-8

N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide

Conditions
Conditions Yield
Multi-step reaction with 4 steps
1: 97 percent / triethylamine / tetrahydrofuran / Ambient temperature
2: 1) TMEDA, sec-Butyllithium (1.35 M in Cyclohexane) / 1) THf, -78 deg C, 1 h, 2) -78 deg C, 1 h; room temperature
3: Diisopropylamine, sec-Butyllithium (1.35 M in cyclohexane) / 1) THF, -78 deg C, 1 h, 2) -78 deg C, 2 h; room temperature
4: CF3CO2H / 48 h / Heating
With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; triethylamine; diisopropylamine; trifluoroacetic acid; In tetrahydrofuran;
N-tert-Butyl-N-methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide
125023-40-7

N-tert-Butyl-N-methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide

N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide
125023-41-8

N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide

Conditions
Conditions Yield
With trifluoroacetic acid; for 48h; Heating;
N-tert-Butyl-N-methyl-2-methoxybenzamide
95330-46-4

N-tert-Butyl-N-methyl-2-methoxybenzamide

N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide
125023-41-8

N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide

Conditions
Conditions Yield
Multi-step reaction with 3 steps
1: 1) TMEDA, sec-Butyllithium (1.35 M in Cyclohexane) / 1) THf, -78 deg C, 1 h, 2) -78 deg C, 1 h; room temperature
2: Diisopropylamine, sec-Butyllithium (1.35 M in cyclohexane) / 1) THF, -78 deg C, 1 h, 2) -78 deg C, 2 h; room temperature
3: CF3CO2H / 48 h / Heating
With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; diisopropylamine; trifluoroacetic acid;
N-tert-Butyl-N-methyl-2-methoxy-6-methylbenzamide
95330-45-3

N-tert-Butyl-N-methyl-2-methoxy-6-methylbenzamide

N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide
125023-41-8

N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1: Diisopropylamine, sec-Butyllithium (1.35 M in cyclohexane) / 1) THF, -78 deg C, 1 h, 2) -78 deg C, 2 h; room temperature
2: CF3CO2H / 48 h / Heating
With sec.-butyllithium; diisopropylamine; trifluoroacetic acid;
p-methoxybenzyl chloride
824-94-2

p-methoxybenzyl chloride

N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide
125023-41-8

N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1: Diisopropylamine, sec-Butyllithium (1.35 M in cyclohexane) / 1) THF, -78 deg C, 1 h, 2) -78 deg C, 2 h; room temperature
2: CF3CO2H / 48 h / Heating
With sec.-butyllithium; diisopropylamine; trifluoroacetic acid;
2-Methoxybenzoyl chloride
21615-34-9

2-Methoxybenzoyl chloride

N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide
125023-41-8

N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide

Conditions
Conditions Yield
Multi-step reaction with 4 steps
1: 97 percent / triethylamine / tetrahydrofuran / Ambient temperature
2: 1) TMEDA, sec-Butyllithium (1.35 M in Cyclohexane) / 1) THf, -78 deg C, 1 h, 2) -78 deg C, 1 h; room temperature
3: Diisopropylamine, sec-Butyllithium (1.35 M in cyclohexane) / 1) THF, -78 deg C, 1 h, 2) -78 deg C, 2 h; room temperature
4: CF3CO2H / 48 h / Heating
With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; triethylamine; diisopropylamine; trifluoroacetic acid; In tetrahydrofuran;
N-tert-Butyl-N-methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide
125023-40-7

N-tert-Butyl-N-methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide

N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide
125023-41-8

N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide

Conditions
Conditions Yield
With trifluoroacetic acid; for 48h; Heating;
N-tert-Butyl-N-methyl-2-methoxybenzamide
95330-46-4

N-tert-Butyl-N-methyl-2-methoxybenzamide

N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide
125023-41-8

N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide

Conditions
Conditions Yield
Multi-step reaction with 3 steps
1: 1) TMEDA, sec-Butyllithium (1.35 M in Cyclohexane) / 1) THf, -78 deg C, 1 h, 2) -78 deg C, 1 h; room temperature
2: Diisopropylamine, sec-Butyllithium (1.35 M in cyclohexane) / 1) THF, -78 deg C, 1 h, 2) -78 deg C, 2 h; room temperature
3: CF3CO2H / 48 h / Heating
With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; diisopropylamine; trifluoroacetic acid;
N-tert-Butyl-N-methyl-2-methoxy-6-methylbenzamide
95330-45-3

N-tert-Butyl-N-methyl-2-methoxy-6-methylbenzamide

N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide
125023-41-8

N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1: Diisopropylamine, sec-Butyllithium (1.35 M in cyclohexane) / 1) THF, -78 deg C, 1 h, 2) -78 deg C, 2 h; room temperature
2: CF3CO2H / 48 h / Heating
With sec.-butyllithium; diisopropylamine; trifluoroacetic acid;
p-methoxybenzyl chloride
824-94-2

p-methoxybenzyl chloride

N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide
125023-41-8

N-Methyl-2-methoxy-6-<2-(4-methoxyphenyl)ethyl>benzamide

Conditions
Conditions Yield
Multi-step reaction with 2 steps
1: Diisopropylamine, sec-Butyllithium (1.35 M in cyclohexane) / 1) THF, -78 deg C, 1 h, 2) -78 deg C, 2 h; room temperature
2: CF3CO2H / 48 h / Heating
With sec.-butyllithium; diisopropylamine; trifluoroacetic acid;

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