A treatment of waste sulfite liquor from sulfite pulp manufacture to recover chemicals and reduce stream pollution. The waste sulfite is treated with lime and precipitates (1) calcium sulfite for use in preparing fresh cooking acid for the sulfite pulp process; and (2) a basic calcium salt of lignin sulfonic acid (lignin sulfonates) that can be pressed and used as a fuel or used as raw material for vanillin, lignin plastics, and other chemicals. The remaining liquor with its BOD reduced 80% is the effluent.