Journal of Organic Chemistry p. 4098 - 4112 (1991)
Update date:2022-07-30
Topics: Synthesis Reactions Experimental Sulfones
Weichert, Andreas
Hoffmann, H. Martin R.
Modified Jones oxidation of 2-(benzenesulfonyl)-2-alken-1-ols and rapid nonnucleophilic workup below 0 deg C yields a variety of α-methylene-β-keto sulfones 4, including crystalline parent 4a and also e-h, which can be stored at -20 deg C without change.I
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