Chemistry of Heterocyclic Compounds p. 522 - 529 (1984)
Update date:2022-07-29
Topics:
Ogle, Ya. V.
Baumane, L. Kh.
Gavar, R. A.
Kadysh, V. P.
Stradyn',Ya. P.
at al.
Free cation radicals, which subsequently undergo deprotonation to neutral radicals and disproportionation to give the starting molecules and pyridinium cations, are formed in the electrochemical oxidation of N-substituted 2,6-dimethyl-3,5-bis(ethoxycarbonyl)-1,3-dihydropyridines on a rotating disk electrode with a ring in solution in acetonitrile.The primary cation radicals were identified by electrochemical generation in a cell placed in the resonator of an EPR spectrometer, and the hyperfine structures of corresponding EPR spectra were studied.
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