Canadian Journal of Chemistry p. 77 - 80 (2006)
Update date:2022-08-04
Topics:
Canty, Allan J.
Devereux
Skelton
White
Methyl(phenoxo)mercury(II) may be obtained from the reaction of methyl(chloro)mercury(II) with silver(I) oxide, followed by addition of phenol. The dominant motif of the structure is a pair of independent MeHgOPh aggregates (Hg-C,O 2.05(2) A, 2.06(1) A (x2); C-Hg-O 176.6(5)°, 176.3(5)°) loosely associated about a quasi-inversion centre by Hg...O interactions (2.702(9) A, 2.719(9) A) to form a dimer (Hg-O-Hg′ 106.0(4)°, 106.5(4)°; O-Hg-O′ 73.0(3)°, 72.6(3)°), the dimer stacking up the short crystallographic c axis (= 6.914(1) A′) at spacings c/2. Vibrational spectroscopic studies are insensitive to the associative interactions.
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