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2628-16-2

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4-Acetoxystyrene 2628-16-2 COA 4-Ethenylphenol acetate Factory PRICE
Cas No: 2628-16-2
USD $ 3.5-5.0 / Kiloliter 5 Kiloliter 3000 Metric Ton/Month Chemwill Asia Co., Ltd. Contact Supplier
4-Acetoxystyrene
Cas No: 2628-16-2
USD $ 1.0-1.0 / Kilogram 1 Kilogram 10 Metric Ton/Month Hangzhou Ocean Chemical Co., Ltd. Contact Supplier
(4-ethenylphenyl) acetate supplier
Cas No: 2628-16-2
USD $ 200.0-200.0 / Kilogram 1 Kilogram 3 Metric Ton/Month Hangzhou ZeErRui Chemical Co., Ltd. Contact Supplier
4-Ethenylphenol acetate
Cas No: 2628-16-2
USD $ 12.0-12.0 / Gram 10 Gram 100 Metric Ton/Year Jinan Finer Chemical Co., Ltd Contact Supplier
4-Ethenylphenol acetate CAS 2628-16-2
Cas No: 2628-16-2
No Data 1 Kilogram 10 Kilogram/Month Hubei Jiutian Bio-medical Technology Co., Ltd Contact Supplier
4-Ethenylphenol acetate
Cas No: 2628-16-2
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
UIV CHEM C10H10O2 hot selling CAS NO.2628-16-2 4-Ethenylphenol acetate
Cas No: 2628-16-2
USD $ 120.0-165.0 / Kilogram 1 Kilogram 100 Metric Ton/Month Yurui(Shanghai)Chemical Co.,Ltd Contact Supplier
High Quality 99% 2628-16-2 4-Ethenylphenol acetate Manufacturer
Cas No: 2628-16-2
USD $ 0.1-0.1 / Gram 1 Gram 100 Metric Ton/Year Xi'an Xszo Chem Co., Ltd. Contact Supplier
4-Ethenylphenol acetate
Cas No: 2628-16-2
No Data No Data 5000 Kilogram/Month Henan Allgreen Chemical Co.,Ltd Contact Supplier
Supply 4-Ethenylphenol Acetate 99% CAS 2628-16-2
Cas No: 2628-16-2
USD $ 110.0-120.0 / Kilogram 1 Kilogram 1000 Kilogram/Day Xi'an Julong Bio-Tech Co., Ltd. Contact Supplier

2628-16-2 Usage

Chemical Properties

clear colorless liquid

Safety Profile

Moderately toxic by ingestion.Slightly toxic by skin contact. An eye irritant. A combustibleliquid. When heated to decomposition it emits acrid smokeand irritating vapors.
InChI:InChI=1/C10H10O2/c1-3-9-4-6-10(7-5-9)12-8(2)11/h3-7H,1H2,2H3

2628-16-2 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
TCI America (A1551)  4-Vinylphenyl Acetate (stabilized with TBC)  >98.0%(GC) 2628-16-2 5g 217.00CNY Detail
TCI America (A1551)  4-Vinylphenyl Acetate (stabilized with TBC)  >98.0%(GC) 2628-16-2 25g 575.00CNY Detail
Alfa Aesar (L11601)  4-Acetoxystyrene, 95%, stab.    2628-16-2 2g 170.0CNY Detail
Alfa Aesar (L11601)  4-Acetoxystyrene, 95%, stab.    2628-16-2 10g 502.0CNY Detail
Aldrich (380547)  4-Acetoxystyrene  96%, contains 200-300 ppm monomethyl ether hydroquinone as inhibitor 2628-16-2 380547-5ML 417.69CNY Detail
Aldrich (380547)  4-Acetoxystyrene  96%, contains 200-300 ppm monomethyl ether hydroquinone as inhibitor 2628-16-2 380547-25ML 1,091.61CNY Detail

2628-16-2SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 11, 2017

Revision Date: Aug 11, 2017

1.Identification

1.1 GHS Product identifier

Product name (4-ethenylphenyl) acetate

1.2 Other means of identification

Product number -
Other names Acetic Acid 4-Vinylphenyl Ester

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:2628-16-2 SDS

2628-16-2Synthetic route

acetic anhydride
108-24-7

acetic anhydride

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
Stage #1: p-Coumaric Acid With bis(1-oxyl-2,2,6,6-tetramethylpiperidin-4-yl)sebacate; potassium acetate In DMF (N,N-dimethyl-formamide) at 150℃; for 2h;
Stage #2: acetic anhydride In DMF (N,N-dimethyl-formamide) at 140℃; for 0.75h; Product distribution / selectivity;
97.5%
Stage #1: p-Coumaric Acid; potassium acetate In ISOPROPYLAMIDE at 135℃; for 3h;
Stage #2: acetic anhydride In ISOPROPYLAMIDE at 20℃; for 0.633333h; Product distribution / selectivity;
71%
4-(1,2-dibromoethyl)phenyl acetate
360068-17-3

4-(1,2-dibromoethyl)phenyl acetate

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
With gallium; bis(cyclopentadienyl)titanium dichloride In tetrahydrofuran at 20℃; for 0.166667h; Inert atmosphere; Ultrasonic irradiation; chemoselective reaction;96%
With bismuth(III) chloride; gallium In tetrahydrofuran at 20℃; for 0.5h;96%
With bismuth(III) chloride; indium In methanol at 20℃; for 0.5h; Sonication; chemoselective reaction;94%
C10H10O2S

C10H10O2S

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
With molybdenum hexacarbonyl In toluene for 2h; Reflux; chemoselective reaction;92%
4'-acetoxyphenylmethylcarbinol
53744-50-6

4'-acetoxyphenylmethylcarbinol

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
With 10H-phenothiazine; 1-ethyl-3-methylimidazolium hydrogensulfate at 150℃; for 6h; Temperature; Reagent/catalyst;90%
With 4-tert-Butylcatechol; potassium hydroxide In N,N-dimethyl acetamide at 100 - 110℃; Reagent/catalyst; Temperature;79.3%
With tert-butylcatechol In toluene at 90℃; for 0.5h; Reagent/catalyst; Temperature; Molecular sieve;78%
With potassium hydrogensulfate at 175 - 200℃;
With acetic anhydride In N,N-dimethyl-formamide at 50℃;
4-Vinylphenol
2628-17-3

4-Vinylphenol

acetyl chloride
75-36-5

acetyl chloride

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
With 10H-phenothiazine; triethylamine In tert-butyl methyl ether at -5 - 20℃; for 1h; Reagent/catalyst; Solvent; Green chemistry;87.7%
With triethylamine In dichloromethane at 0℃; for 3h;69%
With triethylamine In dichloromethane at 20℃;
acetic anhydride
108-24-7

acetic anhydride

4-Vinylphenol
2628-17-3

4-Vinylphenol

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
In N,N-dimethyl acetamide for 0.5h; Heating / reflux;86%
With 10H-phenothiazine; triethylamine In tert-butyl methyl ether at -5 - 20℃; for 1h; Green chemistry;58.6%
With dmap; triethylamine In dichloromethane at 23℃; for 0.5h; Inert atmosphere;24%
With dmap; triethylamine In dichloromethane at 23℃; for 0.5h; Inert atmosphere;24%
at 80℃; under 760.051 Torr; for 2h;80.20 g
vinyl acetate
108-05-4

vinyl acetate

4-chlorophenyl acetate
876-27-7

4-chlorophenyl acetate

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
With manganese; trifluoroacetic acid; [2,2]bipyridinyl; cobalt(II) bromide In pyridine; DMF (N,N-dimethyl-formamide) at 50℃;81%
para-coumaric acid
7400-08-0

para-coumaric acid

acetic anhydride
108-24-7

acetic anhydride

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
Stage #1: para-coumaric acid With 4-methoxy-phenol In water; N,N-dimethyl-formamide at 136℃; for 6h;
Stage #2: acetic anhydride With pyridine In water; N,N-dimethyl-formamide at 30℃; for 0.5h;
75%
4-formylphenyl acetate
878-00-2

4-formylphenyl acetate

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
With Methyltriphenylphosphonium bromide; potassium carbonate In tetrahydrofuran for 6h; Inert atmosphere; Reflux;71%
Multi-step reaction with 2 steps
1: activated Zn powder / dimethylformamide / 50 °C
2: Ac2O / dimethylformamide / 50 °C
View Scheme
4-formylphenyl acetate
878-00-2

4-formylphenyl acetate

Methyltriphenylphosphonium bromide
1779-49-3

Methyltriphenylphosphonium bromide

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
With potassium carbonate In tetrahydrofuran at 70℃; for 24h; Temperature; Wittig Olefination;60.91%
With potassium carbonate In 1,4-dioxane for 16h; Reflux;
Stage #1: Methyltriphenylphosphonium bromide With n-butyllithium In tetrahydrofuran at 0℃; for 0.25h; Inert atmosphere;
Stage #2: 4-formylphenyl acetate In tetrahydrofuran at 0 - 20℃; for 10h; Inert atmosphere;
4-formylphenyl acetate
878-00-2

4-formylphenyl acetate

methyl-triphenylphosphonium iodide
2065-66-9

methyl-triphenylphosphonium iodide

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
With potassium carbonate In tetrahydrofuran Inert atmosphere; Reflux;44%
Stage #1: methyl-triphenylphosphonium iodide With potassium tert-butylate In diethyl ether at 0℃; for 4h;
Stage #2: 4-formylphenyl acetate In diethyl ether at 20℃; for 10h;
4-formylphenyl acetate
878-00-2

4-formylphenyl acetate

methyl-triphenylphosphonium iodide
2065-66-9

methyl-triphenylphosphonium iodide

A

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

B

Triphenylphosphine oxide
791-28-6

Triphenylphosphine oxide

Conditions
ConditionsYield
With Carbowax 6000 (liquid); potassium carbonateA 10%
B n/a
1-acetoxy-4-(1-acetoxy-ethyl)-benzene
68735-72-8

1-acetoxy-4-(1-acetoxy-ethyl)-benzene

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
at 480℃;
at 480℃;
4-acetoxycinnamic acid
27542-85-4

4-acetoxycinnamic acid

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
With quinoline; copper
4'-acetoxyphenylmethylcarbinol
53744-50-6

4'-acetoxyphenylmethylcarbinol

acetic anhydride
108-24-7

acetic anhydride

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
With aluminum oxide; acetic acid at 350℃; under 25 Torr;
4-bromophenyl acetate
1927-95-3

4-bromophenyl acetate

tri-n-butyl(vinyl)tin
7486-35-3

tri-n-butyl(vinyl)tin

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
With pyridine; tetrakis(triphenylphosphine) palladium(0); 2,6-di-tert-butyl-4-methyl-phenol; pyridine hydrogenfluoride 1.) toluene, reflux, 8 h, 2.) toluene, RT, 16 h; Yield given. Multistep reaction;
4'-acetoxyphenylmethylcarbinol
53744-50-6

4'-acetoxyphenylmethylcarbinol

KHSO4

KHSO4

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
at 175 - 200℃;
3-bromo-2-(p-hydroxyphenyl) propionic acid
948888-24-2

3-bromo-2-(p-hydroxyphenyl) propionic acid

acetic anhydride
108-24-7

acetic anhydride

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
Stage #1: 3-bromo-2-(p-hydroxyphenyl) propionic acid; 2-bromo-3-(p-hydroxyphenyl)propanoic acid With potassium carbonate In N,N-dimethyl-formamide at 65℃; for 1h; Heating / reflux;
Stage #2: acetic anhydride In N,N-dimethyl-formamide at 65℃; for 0.25h; Heating / reflux;
4-Ethylphenol
123-07-9

4-Ethylphenol

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: sodium acetate
2: oxygen; chromium oxide-cobalt hydroxide(?)-calcium carbonate catalyst / 145 °C
3: copper oxide-chromium oxide / 130 °C / 102971 Torr / Hydrogenation
4: KHSO4 / 175 - 200 °C
View Scheme
p-ethylphenyl acetate
3245-23-6

p-ethylphenyl acetate

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: oxygen; chromium oxide-cobalt hydroxide(?)-calcium carbonate catalyst / 145 °C
2: copper oxide-chromium oxide / 130 °C / 102971 Torr / Hydrogenation
3: KHSO4 / 175 - 200 °C
View Scheme
4-acetyloxyacetophenone
13031-43-1

4-acetyloxyacetophenone

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: palladium/charcoal; methanol / 30 °C / 5884.06 Torr / Hydrogenation
2: acetic acid; Al2O3 / 350 °C / 25 Torr
View Scheme
Multi-step reaction with 2 steps
1: copper oxide-chromium oxide / 130 °C / 102971 Torr / Hydrogenation
2: KHSO4 / 175 - 200 °C
View Scheme
1-(4-hydroxyphenyl)ethanol
93453-79-3

1-(4-hydroxyphenyl)ethanol

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine; diethyl ether
2: 480 °C
View Scheme
4-Hydroxyacetophenone
99-93-4

4-Hydroxyacetophenone

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: aqueous NaOH
2: palladium/charcoal; methanol / 30 °C / 5884.06 Torr / Hydrogenation
3: acetic acid; Al2O3 / 350 °C / 25 Torr
View Scheme
Multi-step reaction with 3 steps
1: methanol; Raney nickel / 70 - 80 °C / 102971 Torr / Hydrogenation
2: pyridine; diethyl ether
3: 480 °C
View Scheme
Multi-step reaction with 3 steps
1: sodium carbonate / ethyl acetate / 8 h / 20 - 30 °C / Large scale
2: hydrogen; 5%-palladium/activated carbon / toluene / 15 - 20 °C / 6000.6 Torr / Large scale
3: potassium hydroxide; 4-tert-Butylcatechol / N,N-dimethyl acetamide / 100 - 110 °C
View Scheme
Multi-step reaction with 3 steps
1: triethylamine / dichloromethane / 3 h / 0 - 30 °C
2: palladium on activated charcoal; hydrogen / methanol / 5 h / 30 °C / 15001.5 Torr
3: 10H-phenothiazine; 1-ethyl-3-methylimidazolium hydrogensulfate / 6 h / 150 °C
View Scheme
phenol
108-95-2

phenol

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: BF3
2: aqueous NaOH
3: palladium/charcoal; methanol / 30 °C / 5884.06 Torr / Hydrogenation
4: acetic acid; Al2O3 / 350 °C / 25 Torr
View Scheme
vinyl acetate
108-05-4

vinyl acetate

4-bromophenyl acetate
1927-95-3

4-bromophenyl acetate

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
With manganese; trifluoroacetic acid; [2,2]bipyridinyl; cobalt(II) bromide In pyridine; DMF (N,N-dimethyl-formamide) at 50℃; for 0.5h;
4-hydroxy-benzaldehyde
123-08-0

4-hydroxy-benzaldehyde

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
2: potassium carbonate; Methyltriphenylphosphonium bromide / tetrahydrofuran / 6 h / Inert atmosphere; Reflux
View Scheme
Multi-step reaction with 2 steps
1.1: sodium hydride / dimethyl sulfoxide / 0.25 h / Inert atmosphere; Cooling with ice
1.2: 5 h / 23 °C / Inert atmosphere
2.1: triethylamine; dmap / dichloromethane / 0.5 h / 23 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1.1: sodium hydride / dimethyl sulfoxide / 0.25 h / Inert atmosphere
1.2: 5 h / 23 °C
2.1: triethylamine; dmap / dichloromethane / 0.5 h / 23 °C / Inert atmosphere
View Scheme
para-coumaric acid
7400-08-0

para-coumaric acid

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: pyridine; glycine / 8 h / 140 °C
2: 2 h / 80 °C / 760.05 Torr
View Scheme
4-(oxiran-2-yl)phenyl acetate
86952-89-8

4-(oxiran-2-yl)phenyl acetate

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium thioacyanate
2: molybdenum hexacarbonyl / toluene / 2 h / Reflux
View Scheme
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

diphenylolpropane diglycidyl ether
1675-54-3

diphenylolpropane diglycidyl ether

C41H44O8

C41H44O8

Conditions
ConditionsYield
dmap at 85℃; for 60h;100%
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

2-hydroxy-2-methylpropanenitrile
75-86-5

2-hydroxy-2-methylpropanenitrile

2-(4-acetoxyphenyl)propanenitrile
1132795-53-9

2-(4-acetoxyphenyl)propanenitrile

Conditions
ConditionsYield
With 3-[bis-(4-methoxy-phenyl)-phosphanyl]-2H-isoquinolin-1-one; N-{6-[bis-(4-methoxy-phenyl)-phosphanyl]-pyridin-2-yl}-2,2-dimethyl-propionamide; bis(1,5-cyclooctadiene)nickel (0) In toluene at 35℃; for 40h; Inert atmosphere; regioselective reaction;100%
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

bis(trifluoroacetyl)peroxide
383-73-3

bis(trifluoroacetyl)peroxide

C13H10F6O4

C13H10F6O4

Conditions
ConditionsYield
In dichloromethane at 40℃; for 1h;100%
bis(heptafluorobutyryl) peroxide
336-64-1

bis(heptafluorobutyryl) peroxide

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

C17H10F14O4

C17H10F14O4

Conditions
ConditionsYield
In dichloromethane at 40℃; for 1h;100%
2-carbonyl-3-butenenitrile
60556-87-8

2-carbonyl-3-butenenitrile

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

2-[(4-acetyloxy)phenyl]-3,4-dihydro-2H-pyran-6-carbonitrile

2-[(4-acetyloxy)phenyl]-3,4-dihydro-2H-pyran-6-carbonitrile

Conditions
ConditionsYield
In acetonitrile at 81℃; for 24h; hetero-Diels-Alder cycloaddition;99%
formaldehyd
50-00-0

formaldehyd

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

4-(4-acetoxyphenyl)-1,3-dioxane

4-(4-acetoxyphenyl)-1,3-dioxane

Conditions
ConditionsYield
With 2,6-di-tert-butylphenoxy(difluoro)borane In 1,4-dioxane at 100℃; for 12h; Prins reaction;99%
With bismuth(lll) trifluoromethanesulfonate In acetonitrile for 10h; Prins reaction; Heating;77%
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

4-(1-fluoroethyl)phenyl acetate

4-(1-fluoroethyl)phenyl acetate

Conditions
ConditionsYield
With triethylsilane; tetrakis(triphenylphosphine) palladium(0); Selectfluor In acetonitrile at 0℃; for 2h; regioselective reaction;99%
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

p-ethylphenyl acetate
3245-23-6

p-ethylphenyl acetate

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen at 20℃; for 18h; Sealed tube;99%
With 1% Pd on activated carbon; hydrogen In water at 20℃; under 760.051 Torr; for 2h; Reagent/catalyst; Green chemistry; chemoselective reaction;99%
With hydrogen In toluene at 40℃; under 2250.23 Torr; Catalytic behavior; Reagent/catalyst; Schlenk technique; Glovebox;
With ammonia borane In water at 24.84℃; for 4h; Sonication; Green chemistry;
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

(E)-4,4’-diacetoxystilbene
47241-75-8

(E)-4,4’-diacetoxystilbene

Conditions
ConditionsYield
RuCl2(=CHPh)[1,3-ImH2]P(Cy)3 In dichloromethane at 40℃; for 2h;98%
With Hoveyda-Grubbs catalyst second generation In dichloromethane at 40℃; for 15h;93%
With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride In methanol; dichloromethane; water at 45℃; for 5h; Ionic liquid; Inert atmosphere; Catalyst solution in CH2Cl2/BMIM incapsulated within polydimethylsiloxane thimble;80%
(1,3-dimesitylimidazolin-2-ylidene)(C2H4)RuCl2; (p-cymene)RuCl2 In toluene at 85℃; for 2h;100 % Turnov.
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Umemoto's reagent

Umemoto's reagent

3,3,3-trifluoro-1-(4-acetoxyphenyl)-1-propanol
1417820-87-1

3,3,3-trifluoro-1-(4-acetoxyphenyl)-1-propanol

Conditions
ConditionsYield
With tris[2-phenylpyridinato-C2,N]iridium(III); water In acetone at 20℃; for 3h; Schlenk technique; Inert atmosphere; Irradiation; regioselective reaction;98%
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

2-Mercaptobenzothiazole
149-30-4

2-Mercaptobenzothiazole

C17H15NO2S2
1446094-31-0

C17H15NO2S2

Conditions
ConditionsYield
With trifluoroacetic acid In dichloromethane at 20℃; regioselective reaction;98%
ethyl 4-[7-bromo-1-(2-ethoxy-2-oxoethyl)-1H-indol-3-yl]butanoate
908133-83-5

ethyl 4-[7-bromo-1-(2-ethoxy-2-oxoethyl)-1H-indol-3-yl]butanoate

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

C28H31NO6

C28H31NO6

Conditions
ConditionsYield
With dicyclohexylmethylamine; triethylamine In 1,4-dioxane; hexane at 100℃; for 3h; Heck Reaction; Inert atmosphere;98%
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

4-(1,2-dihydroxyethyl)phenyl acetate
439584-65-3

4-(1,2-dihydroxyethyl)phenyl acetate

Conditions
ConditionsYield
With osmium(VIII) oxide; 4-methylmorpholine N-oxide In water; acetone at 0 - 20℃; for 4h; Inert atmosphere;97%
Stage #1: p-acetoxystyrene With sodium periodate; acetic acid; lithium bromide at 95℃; for 18h; Prevost-Woodward reaction;
Stage #2: With potassium carbonate In methanol at 25℃; for 24h;
With Quinuclidine; osmium(VIII) oxide; tert-butyl alcohol In acetone at 25℃; for 12h;
aqueous DMF

aqueous DMF

4-bromocyclobutabenzene

4-bromocyclobutabenzene

[(4-benzocyclobutenyl)vinyl] phenol

[(4-benzocyclobutenyl)vinyl] phenol

[(4-benzocyclobutenyl)-vinyl] phenyl acetate

[(4-benzocyclobutenyl)-vinyl] phenyl acetate

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

tris-(o-tolyl)phosphine
6163-58-2

tris-(o-tolyl)phosphine

[(4-cyclobutenyl)vinyl] phenol

[(4-cyclobutenyl)vinyl] phenol

Conditions
ConditionsYield
With potassium acetate; palladium diacetate In water; N,N-dimethyl-formamide97%
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

4-bromo-5, 5, 5-trifluoropentan-1-ol

4-bromo-5, 5, 5-trifluoropentan-1-ol

(E)-4-(6-hydroxy-3-(trifluoromethyl)hex-1-en-1-yl)phenyl acetate

(E)-4-(6-hydroxy-3-(trifluoromethyl)hex-1-en-1-yl)phenyl acetate

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; potassium acetate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene at 80℃; for 16h; Heck Reaction; Schlenk technique; Inert atmosphere;97%
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

4-nitrobenzaldehyde oxime
1129-37-9

4-nitrobenzaldehyde oxime

C17H14N2O5

C17H14N2O5

Conditions
ConditionsYield
With sodium hypochlorite In dichloromethane; water97%
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

2-bromo-1-(4-methylpent-3-en-1-yl)-1H-benzo[d]imidazole

2-bromo-1-(4-methylpent-3-en-1-yl)-1H-benzo[d]imidazole

(E)-4-(3-(2,3-dihydro-1H-benzo[d]pyrrolo[1,2-a]imidazol-3-yl)-3-methylbut-1-en-1-yl)phenyl acetate

(E)-4-(3-(2,3-dihydro-1H-benzo[d]pyrrolo[1,2-a]imidazol-3-yl)-3-methylbut-1-en-1-yl)phenyl acetate

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In 1,4-dioxane for 24h; Schlenk technique; Inert atmosphere; Irradiation; stereoselective reaction;97%
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

4-Vinylphenol
2628-17-3

4-Vinylphenol

Conditions
ConditionsYield
With ethanol; sodium hydroxide at 20℃; for 4h; Inert atmosphere;96%
With sodium hydroxide In tetrahydrofuran; water at 20℃; for 4h; Cooling with ice; Inert atmosphere; Schlenk technique;96%
With sodium hydroxide In ethanol at 20℃; for 4h; Inert atmosphere;96%
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

4-(oxiran-2-yl)phenyl acetate
86952-89-8

4-(oxiran-2-yl)phenyl acetate

Conditions
ConditionsYield
Stage #1: p-acetoxystyrene With tris(μ-oxo)di[(1,4,7-trimethyl-1,4,7-triazanonane)manganese(IV)] hexafluorophosphate; scandium tris(trifluoromethanesulfonate) In acetonitrile at 20℃; for 0.166667h; Sealed tube;
Stage #2: With dihydrogen peroxide In water; acetonitrile for 0.05h; Sealed tube;
96%
With oxone(R); PEG-supported α,α,α-trifluoroacetophenone; sodium hydrogencarbonate In 1,4-dioxane; water at 20℃; for 0.0833333h;84%
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 0 - 20℃; for 24h;75%
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

methyl iodide
74-88-4

methyl iodide

4-Methoxystyrene
637-69-4

4-Methoxystyrene

Conditions
ConditionsYield
With potassium hydroxide In water; acetone at 20℃; for 124h;96%
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

C11H9BrFNO4S2

C11H9BrFNO4S2

C21H17NO4S

C21H17NO4S

Conditions
ConditionsYield
With copper(l) iodide; bathophenanthroline; sodium carbonate In dichloromethane at 100℃; for 60h; Sealed tube; Inert atmosphere;96%
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

4-acetyloxyacetophenone
13031-43-1

4-acetyloxyacetophenone

Conditions
ConditionsYield
With perchloric acid; oxygen; palladium diacetate; p-benzoquinone; sodium nitrite In methanol; water at 20℃; for 5h; Wacker Oxidation; Schlenk technique; Sealed tube; Green chemistry;95%
With iron(II) chloride In ethanol at 80℃; for 4h;88%
With tert.-butylhydroperoxide; palladium(II) bis(diketonate) In benzene at 56℃;84%
iodobenzene
591-50-4

iodobenzene

p-acetoxystyrene
2628-16-2

p-acetoxystyrene

Trans-acetic acid 4-styrylphenyl ester
93022-30-1, 13041-73-1

Trans-acetic acid 4-styrylphenyl ester

Conditions
ConditionsYield
With triethylamine; poly{bis[(N-iPr-acrylamide)5-co-((4-vinylphenyl)PPh2)]PdCl2} In toluene at 100℃; for 20h; Heck reaction;95%
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

3,4-dimethoxybenzenediazonium tetrafluoroborate

3,4-dimethoxybenzenediazonium tetrafluoroborate

(E)-1-(4'-acetoxyphenyl)-2-(3,4-dimethoxyphenyl)ethene
880354-47-2

(E)-1-(4'-acetoxyphenyl)-2-(3,4-dimethoxyphenyl)ethene

Conditions
ConditionsYield
With palladium diacetate; sodium acetate In benzonitrile at 25℃; Heck arylation reaction;95%
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

3,4,5-trimethoxybenzenediazonium tetrafluoroborate

3,4,5-trimethoxybenzenediazonium tetrafluoroborate

(E)-1-(4-acetoxyphenyl)-2-(2,3,4-trimethoxyphenyl)ethene
134029-69-9

(E)-1-(4-acetoxyphenyl)-2-(2,3,4-trimethoxyphenyl)ethene

Conditions
ConditionsYield
With Pd2(dba)4; sodium acetate In benzonitrile at 25℃; for 1h; Heck arylation reaction;95%
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

3,5-dimethoxybenzenediazonium tetrafluoroborate
72470-95-2

3,5-dimethoxybenzenediazonium tetrafluoroborate

(E)-1-(4'-acetoxyphenyl)-2-(3,5-dimethoxyphenyl)ethene
18259-14-8, 63366-83-6

(E)-1-(4'-acetoxyphenyl)-2-(3,5-dimethoxyphenyl)ethene

Conditions
ConditionsYield
With palladium diacetate; sodium acetate In benzonitrile at 25℃; for 3h; Heck arylation reaction;95%
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

4-hydroxybenzenediazonium tetrafluoroborate

4-hydroxybenzenediazonium tetrafluoroborate

(E)-1-acetyloxy-4-(4-hydroxystyryl)benzene

(E)-1-acetyloxy-4-(4-hydroxystyryl)benzene

Conditions
ConditionsYield
With sodium acetate; palladium diacetate In methanol at 20℃; for 12h; Heck Reaction; Inert atmosphere;95%
p-acetoxystyrene
2628-16-2

p-acetoxystyrene

4-ethoxy-4H-1,4-benzoxaphosphorin-4-oxide
1473394-59-0

4-ethoxy-4H-1,4-benzoxaphosphorin-4-oxide

(E)-3-[2-(4-acetoxyphenyl)ethenyl]-4-ethoxy-4H-1,4-benzoxaphosphorin-4-oxide
1473394-82-9

(E)-3-[2-(4-acetoxyphenyl)ethenyl]-4-ethoxy-4H-1,4-benzoxaphosphorin-4-oxide

Conditions
ConditionsYield
With copper diacetate; palladium diacetate; trimethylpyruvic acid; silver carbonate at 80℃; for 6h;95%
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