Journal of Organic Chemistry p. 423 - 434 (2019)
Update date:2022-08-11
Topics:
Liu, Lihua
Bao, Xifei
Xiao, Hua
Li, Junlan
Ye, Feifan
Wang, Chaoqin
Cai, Qinhua
Fan, Shilu
A general and practical method for copper-catalyzed cross-coupling of allyl phosphates with stable perfluoroalkylzinc reagents has been developed. The reaction proceeds under mild reaction conditions with high efficiency, good functional group tolerance, and high regio- A nd stereoselectivities and provides general, straightforward, and useful access to allyl-perfluoroalkyl compounds. Preliminary mechanistic studies reveal that the allyl copper intermediate may be involved in the catalytic cycle.
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