Russian Chemical Bulletin p. 1242 - 1244 (1994)
Update date:2022-08-11
Topics:
Lomakova, I.V.
Patrikeeva, N. B.
Domrachev, G. A.
Petrov, B. I.
The reaction between (Et3Ge)2Cd and TiCl4 in the presence of α,α'-bipyridyl afforded a compound with a Ge-Cd-Ti group.This compound was characterized by IR and ESR spectroscopy.Thermal decomposition of this compound at 130 and 160 deg C and its interaction with gaseous HCl were studied.A novel complex, (Et3Ge)2Cd*bpy, was obtained as a by-product of the reaction, and some its physicochemical characteristics were determined.Based on the experimental results, a scheme for the interaction of (Et3Ge)2Cd with TiCl4 has been suggested. - Key words: mixed organo-Cd, Ti compounds.
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