Tetrahedron Letters p. 3361 - 3364 (1997)
Update date:2022-08-11
Topics:
Canne, Lynne E.
Winston, Rachel L.
Kent, Stephen B. H.
The synthesis of a versatile handle for the purification of synthetic peptides is described. The Boc-aminoethylsulfonylethyloxycarbonyl handle is coupled to the NH2-terminus of the resin-bound peptide. Removal of the Boc group affords a free amine which can be derivatized with any of a variety of functionalities. Cleavage from the resin gives a peptide functionalized for covalent chemoselective reaction with the column support. Desired full length peptide is eluted from the column by cleavage of the handle by treatment with base.
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