Journal of Fluorine Chemistry p. 25 - 30 (1994)
Update date:2022-08-17
Topics:
Saloutin, V. I.
Skryabina, Z. E.
Burgart, Y. V.
Chupakhin, O. N.
Font-Altaba, M.
et al.
5,7-Trifluoromethyl-6-fluoro-2,3-dihydro-1H-1,4-diazepine has been prepared by the reaction of perfluoropent-2-ene (or 2-amino-4-iminoperfluoropent-2-ene) with ethylenediamine.Both perfluoropent-2-ene and 2-amino-4-iminoperfluoropent-2-ene were found to react with diethylenetriamine to form 1,9-trifluoromethyl-3,4,6,7-tetrahydro-2H-pyrazino<1,2-a>pyrazine (established by X-ray study).Some salts and the complex with BF3 of this bicyclic compound are described.
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