Journal of Physical Chemistry p. 2099 - 2109 (1986)
Update date:2022-08-29
Topics:
Ase, P.
Bock, W.
Snelson, A.
Methyl radicals, generated by the pyrolysis of azomethane and/or methyl iodide, were allowed to interact with matrices of Ar + 10percent O2 and the products isolated.IR spectra were obtained for species containing the following isotopically labeled groups: CH3, 13CH3, CD3, 16O2, 18O2 and 16O(18)O.From these spectra, the methylperoxy radical and its dimer, dimethyltetroxide, were identified and vibrational assignments made.Irradiation of CH3O2 at ca. 254 nm resulted in its photodissociation.The nature of this process in the matrix is discussed.
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