Journal of Fluorine Chemistry p. 19 - 26 (1995)
Update date:2022-08-22
Topics:
Achilefu, Samuel
Mansuy, Laurence
Selve, Claude
Thiebaut, Sylvie
An efficient and convenient procedure for the synthesis of 2-perfluoroalkyl ethanoic acids by direct oxidation of 2-perfluoroalkyl ethanols with Jones' reagent (CrO3/H2SO4) is described.Treatment of the acids with aqueous sodium hydroxide gave 3-perfluoroalkyl, 3-fluoro-2,3-propenyl carboxylic acids wich may be used for the preparation of the corresponding chlorides and amides. - Keywords: Synthesis; 2-Perfluoroalkyl ethanoic acids; Jones' reagent; NMR spectroscopy; IR spectroscopy
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