2-(azidomethyl)benzoyl Chloride

Base Information

Chemical Name:2-(azidomethyl)benzoyl Chloride
CAS No.:289712-58-9
Molecular Formula:C8H6ClN3O
Molecular Weight:195.608
Hs Code.:
DSSTox Substance ID:DTXSID801303819
Nikkaji Number:J1.467.728C

Synonyms:2-(azidomethyl)benzoyl Chloride;SCHEMBL14699642;QSMKHJFDTBZVKR-UHFFFAOYSA-N;DTXSID801303819;2-(Azidomethyl)benzoic acid chloride;289712-58-9

Suppliers and Price of 2-(azidomethyl)benzoyl Chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2-(azidomethyl)benzoyl Chloride

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:195.0199395
Heavy Atom Count:13
Complexity:238

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)CN=[N+]=[N-])C(=O)Cl

Technology Process of 2-(azidomethyl)benzoyl Chloride

There total 6 articles about 2-(azidomethyl)benzoyl Chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 289712-57-8
2-(azidomethyl)benzoic acid

: 289712-58-9
2-(azidomethyl)benzoyl chloride

Guidance literature:: With thionyl chloride; for 1h; Heating;
DOI:10.1016/S0040-4039(00)02183-3

Reference yield:

: 89-71-4
2-Methyl-benzoic acid methyl ester

: 289712-58-9
2-(azidomethyl)benzoyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: NBS / benzoyl peroxide / CCl₄ / 24 h / Heating

2: 4.58 g / NaN₃ / ethanol / 48 h / 20 °C

3: 97 percent / LiOH*H₂O; H₂O / tetrahydrofuran / 60 h / 20 °C

4: 97 percent / thionyl chloride / CHCl₃ / 5 h / Heating

With lithium hydroxide; N-Bromosuccinimide; thionyl chloride; sodium azide; water; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; ethanol; chloroform;
DOI:10.1021/jo015987h

Reference yield:

: 329781-57-9
methyl 2-(azidomethyl) benzoate

: 289712-58-9
2-(azidomethyl)benzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH / methanol; H₂O / 3 h

2: SOCl₂; N,N-dimethylfomamide / 2 h / 60 °C

With sodium hydroxide; thionyl chloride; N,N-dimethyl-formamide; In methanol; water;
DOI:10.1081/SCC-120014042