Technology Process of Dibenzyl prop-2-en-1-ylphosphonate
There total 3 articles about Dibenzyl prop-2-en-1-ylphosphonate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
n-butyllithium;
In
diethyl ether; hexane;
at 20 ℃;
for 4h;
DOI:10.1021/ol702082k
- Guidance literature:
-
Dibenzyl phosphite;
With
n-butyllithium;
In
diethyl ether; hexane;
at -78 ℃;
for 1h;
allyl bromide;
In
diethyl ether; hexane;
at -78 - 20 ℃;
for 5h;
DOI:10.1002/ejoc.201600333
- Guidance literature:
-
Allylphosphonsaeure, Phenyldiazomethan;
