[RuCl(1-methyl-2-(o-(methylthio)phenylazo)imidazole-κN,N',S)(1-methyl-2-(o-(methylthio)phenylazo)imidazole-κN,N)]ClO4

Base Information

Chemical Name:[RuCl(1-methyl-2-(o-(methylthio)phenylazo)imidazole-κN,N',S)(1-methyl-2-(o-(methylthio)phenylazo)imidazole-κN,N)]ClO4
CAS No.:1192621-86-5
Molecular Formula:C₂₂H₂₄ClN₈RuS₂*ClO₄
Molecular Weight:700.592
Hs Code.:

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Chemical Property of [RuCl(1-methyl-2-(o-(methylthio)phenylazo)imidazole-κN,N',S)(1-methyl-2-(o-(methylthio)phenylazo)imidazole-κN,N)]ClO4

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Technology Process of [RuCl(1-methyl-2-(o-(methylthio)phenylazo)imidazole-κN,N',S)(1-methyl-2-(o-(methylthio)phenylazo)imidazole-κN,N)]ClO4

There total 1 articles about [RuCl(1-methyl-2-(o-(methylthio)phenylazo)imidazole-κN,N',S)(1-methyl-2-(o-(methylthio)phenylazo)imidazole-κN,N)]ClO4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14898-67-0
ruthenium(III) chloride trihydrate

: 887114-97-8
1-methyl-2-[o-(methylsulfanyl)phenylazo]imidazole

: sodium perchlorate

: 1192621-86-5
[RuCl(1-methyl-2-(o-(methylthio)phenylazo)imidazole-κN,N',S)(1-methyl-2-(o-(methylthio)phenylazo)imidazole-κN,N)]ClO4

Guidance literature:: In methanol; water; (N2); soln. of RuCl3*3H2O in MeOH refluxed for 1 h, soln. of imidazole deriv. in MeOH added, mixt. refluxed for 4 h, evapn. under vac., residue dissolved in MeOH, aq. soln. of NaClO4 added; ppt. filtered off, washed with cold water, dried under vac. over P2O5, dissolved in CH2Cl2, column chromy. (silica, C6H6/CH3CN 5/1), appropriateeleuate slowly evapd. in air; elem. anal.;
DOI:10.1016/j.jorganchem.2009.06.021