Methanone, (4-bromophenyl)(3-phenyloxiranyl)-

Base Information

Chemical Name:Methanone, (4-bromophenyl)(3-phenyloxiranyl)-
CAS No.:29425-81-8
Molecular Formula:C15H11BrO2
Molecular Weight:303.155
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methanone, (4-bromophenyl)(3-phenyloxiranyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Methanone, (4-bromophenyl)(3-phenyloxiranyl)-

There total 8 articles about Methanone, (4-bromophenyl)(3-phenyloxiranyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 72758-69-1,2403-27-2,22966-23-0
(E)-1-(4-bromophenyl)-3-phenylprop-2-en-1-one

: 29425-81-8
(4-bromophenyl)(3-phenyloxiran-2-yl)methanone

Guidance literature:: (E)-1-(4-bromophenyl)-3-phenylprop-2-en-1-one; With diethylzinc; Phenyl-(4-phenyl-quinazolin-2-yl)-methanol; In tetrahydrofuran; hexane; at 20 ℃; for 0.5h; Sealed tube; Inert atmosphere;

With p-cumenyl hydroperoxide; In tetrahydrofuran; hexane; toluene; at -20 ℃; for 24h; enantioselective reaction; Sealed tube; Inert atmosphere;
DOI:10.1055/s-0035-1561584

Reference yield: 88.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 1122-91-4
4-bromo-benzaldehyde

: 29425-81-8
(4-bromophenyl)(3-phenyloxiran-2-yl)methanone

Guidance literature:: With tert.-butylhydroperoxide; potassium carbonate; In water; acetonitrile; at 100 ℃; for 12h;
DOI:10.1039/c4cc09260k

Reference yield:

: 2403-27-2
1-(4-bromophenyl)-3-phenyl-2-propen-1-one

: 29425-81-8,32157-71-4,67175-56-8
1-p-Brombenzoyl-2-phenyl-ethylenoxid

: C₁₅H₁₁BrO₂

Guidance literature:: 1-(4-bromophenyl)-3-phenyl-2-propen-1-one; With tris(bis(trimethylsilyl)amido)ytterbium(III); 1,8-diazabicyclo[5.4.0]undec-7-ene; (4R-trans)-2,2-dimethyl-α,α,α',α'-tetra{bis(3,5-trifluoromethyl)phenyl}-1,3-dioxolane-4,5-dimethanol; In acetonitrile; at -30 ℃; for 0.5h; Inert atmosphere;

With tert.-butylhydroperoxide; In decane; acetonitrile; at -30 ℃; for 16h; Overall yield = 98 percent; enantioselective reaction; Inert atmosphere; Sealed tube;