Technology Process of 6,9,12-Hexadecatrienoic acid, (6Z,9Z,12Z)-
There total 5 articles about 6,9,12-Hexadecatrienoic acid, (6Z,9Z,12Z)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium hydroxide monohydrate;
In
tetrahydrofuran; water;
at 20 ℃;
for 18h;
Inert atmosphere;
DOI:10.1021/acs.joc.0c02726
- Guidance literature:
-
Multi-step reaction with 3 steps
1: copper(l) iodide; sodium iodide; caesium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere
2: nickel(II) acetate tetrahydrate; sodium tetrahydroborate; hydrogen; ethylenediamine / ethanol / 3 h / 0 - 20 °C
3: lithium hydroxide monohydrate / tetrahydrofuran; water / 18 h / 20 °C / Inert atmosphere
With
sodium tetrahydroborate; copper(l) iodide; lithium hydroxide monohydrate; hydrogen; nickel(II) acetate tetrahydrate; caesium carbonate; ethylenediamine; sodium iodide;
In
tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/acs.joc.0c02726
- Guidance literature:
-
Multi-step reaction with 2 steps
1: nickel(II) acetate tetrahydrate; sodium tetrahydroborate; hydrogen; ethylenediamine / ethanol / 3 h / 0 - 20 °C
2: lithium hydroxide monohydrate / tetrahydrofuran; water / 18 h / 20 °C / Inert atmosphere
With
sodium tetrahydroborate; lithium hydroxide monohydrate; hydrogen; nickel(II) acetate tetrahydrate; ethylenediamine;
In
tetrahydrofuran; ethanol; water;
DOI:10.1021/acs.joc.0c02726
