1,2-Dichloro-1,2-dimethyl-1,2-diphenyldisilane

Base Information

• Chemical Name: 1,2-Dichloro-1,2-dimethyl-1,2-diphenyldisilane
• CAS No.: 29442-41-9
• Molecular Formula: C14H16Cl2Si2
• Molecular Weight: 311.358
• DSSTox Substance ID: DTXSID60565347
• Nikkaji Number: J947.135I
• Mol file: 29442-41-9.mol

Synonyms:1,2-Dichloro-1,2-dimethyl-1,2-diphenyldisilane;29442-41-9;SCHEMBL9383203;DTXSID60565347;1,2-dimethyl-1,2-diphenyl-1,2-dichlorodisilane

Chemical Property of 1,2-Dichloro-1,2-dimethyl-1,2-diphenyldisilane

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 3
• Exact Mass: 310.0167590
• Heavy Atom Count: 18
• Complexity: 247

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C[Si](C1=CC=CC=C1)([Si](C)(C2=CC=CC=C2)Cl)Cl

Technology Process of 1,2-Dichloro-1,2-dimethyl-1,2-diphenyldisilane

There total 8 articles about 1,2-Dichloro-1,2-dimethyl-1,2-diphenyldisilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1,2-bis(diethylamino)-1,1-dimethyl-2,2-diphenyldisilane → 1,2-dichloro-1,2-dimethyl-1,2-diphenyldisilane (29442-41-9)

Guidance literature:

With acetyl chloride; In diethyl ether; at 0 ℃; for 2h;

DOI:10.1016/0022-328X(96)06239-0

Reference yield: 79.0%

1,2-dimethyl-1,2-diphenyldisilane (18410-59-8) → 1,2-dichloro-1,2-dimethyl-1,2-diphenyldisilane (29442-41-9)

Guidance literature:

With copper(l) iodide; copper dichloride; In diethyl ether;

DOI:10.1016/S0022-328X(03)00254-7

Reference yield: 59.0%

1,2-dimethyl-1,2-diphenyldisilane (18410-59-8) → 1,2-dichloro-1,2-dimethyl-1,2-diphenyldisilane (29442-41-9) + 1,2-dimethyl-1,2-diphenyl chlorodisilane

Guidance literature:

With copper(l) iodide; copper dichloride; In diethyl ether;

DOI:10.1016/S0022-328X(03)00254-7

upstream raw materials:

1,2-dimethyl-1,2-diphenyldisilane

1,1,2,2-tetrachloro-1,2-dimethyldisilane

phenylmagnesium chloride

chloro(N,N-diethylamino)diphenylsilane

Downstream raw materials:

cis-1,2-methyl-1,2-diphenyl-1,2-disilacyclohexane

trans-1,2-methyl-1,2-diphenyl-1,2-disilacyclohexane

1,2-difluoro-1,2-dimethyl-1,2-diphenyl-disilane

1,2-dimethyl-1,2-diphenyldivinyldisilane