8b-diethylamino-10a-methyl-2,10b-diphenyl-10a,10b-dihydro-8bH-benzo[e]cyclobuta[c][1,3,4]oxadiazolo[3,2-a]pyridine-9,10-dicarboxylic acid diethyl ester

Base Information

• Chemical Name: 8b-diethylamino-10a-methyl-2,10b-diphenyl-10a,10b-dihydro-8bH-benzo[e]cyclobuta[c][1,3,4]oxadiazolo[3,2-a]pyridine-9,10-dicarboxylic acid diethyl ester
• CAS No.: 72627-59-9
• Molecular Formula: C₃₅H₃₇N₃O₅
• Molecular Weight: 579.696

Synonyms:

Chemical Property of 8b-diethylamino-10a-methyl-2,10b-diphenyl-10a,10b-dihydro-8bH-benzo[e]cyclobuta[c][1,3,4]oxadiazolo[3,2-a]pyridine-9,10-dicarboxylic acid diethyl ester

Chemical Property:

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MSDS Files:

Useful:

Technology Process of 8b-diethylamino-10a-methyl-2,10b-diphenyl-10a,10b-dihydro-8bH-benzo[e]cyclobuta[c][1,3,4]oxadiazolo[3,2-a]pyridine-9,10-dicarboxylic acid diethyl ester

There total 3 articles about 8b-diethylamino-10a-methyl-2,10b-diphenyl-10a,10b-dihydro-8bH-benzo[e]cyclobuta[c][1,3,4]oxadiazolo[3,2-a]pyridine-9,10-dicarboxylic acid diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3,5-triphenyl-1,3,4-oxadiazolium perchlorate → 8b-diethylamino-10a-methyl-2,10b-diphenyl-10a,10b-dihydro-8bH-benzo[e]cyclobuta[c][1,3,4]oxadiazolo[3,2-a]pyridine-9,10-dicarboxylic acid diethyl ester (72627-59-9)

Guidance literature:

Multi-step reaction with 2 steps

1: acetone

2: acetonitrile

In acetone; acetonitrile;

Reference yield:

methyl(diethylamino)acetylene (4231-35-0) → 8b-diethylamino-10a-methyl-2,10b-diphenyl-10a,10b-dihydro-8bH-benzo[e]cyclobuta[c][1,3,4]oxadiazolo[3,2-a]pyridine-9,10-dicarboxylic acid diethyl ester (72627-59-9)

Guidance literature:

Multi-step reaction with 2 steps

1: acetone

2: acetonitrile

In acetone; acetonitrile;

Reference yield:

diethyl-(4-methyl-2,3a-diphenyl-3aH-[1,3,4]oxadiazolo[3,2-a]quinolin-5-yl)-amine (72606-82-7) + acetylenedicarboxylic acid diethyl ester (762-21-0) → 8b-diethylamino-10a-methyl-2,10b-diphenyl-10a,10b-dihydro-8bH-benzo[e]cyclobuta[c][1,3,4]oxadiazolo[3,2-a]pyridine-9,10-dicarboxylic acid diethyl ester (72627-59-9)

Guidance literature:

In acetonitrile;

upstream raw materials:

diethyl-(4-methyl-2,3a-diphenyl-3aH-[1,3,4]oxadiazolo[3,2-a]quinolin-5-yl)-amine

acetylenedicarboxylic acid diethyl ester

methyl(diethylamino)acetylene

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