4-Chloro-N-hydroxy-N-(4-methylphenyl)benzamide

Base Information

Chemical Name:4-Chloro-N-hydroxy-N-(4-methylphenyl)benzamide
CAS No.:29556-29-4
Molecular Formula:C14H12ClNO2
Molecular Weight:261.708
Hs Code.:
DSSTox Substance ID:DTXSID60577501
Nikkaji Number:J462.800D
Wikidata:Q82467529
Mol file:29556-29-4.mol

Synonyms:4-Chloro-N-hydroxy-N-(4-methylphenyl)benzamide;29556-29-4;DTXSID60577501;N-p-tolyl-4-chlorobenzohydroxamic acid

Suppliers and Price of 4-Chloro-N-hydroxy-N-(4-methylphenyl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Chloro-N-hydroxy-N-(4-methylphenyl)benzamide

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:261.0556563
Heavy Atom Count:18
Complexity:282

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)N(C(=O)C2=CC=C(C=C2)Cl)O

Technology Process of 4-Chloro-N-hydroxy-N-(4-methylphenyl)benzamide

There total 1 articles about 4-Chloro-N-hydroxy-N-(4-methylphenyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29556-29-4
N-p-Tolyl-p-chlorobenzohydroxamic acid

Guidance literature:: N-p-Tolyl-hydroxylamin, 4-Chlor-benzoylchlorid, Ae., Py., <0grad;
DOI:10.1021/je60015a036

Reference yield:

: 29556-29-4
N-p-Tolyl-p-chlorobenzohydroxamic acid

: 623-10-9
N-(4-methylphenyl)hydroxylamine

: 3686-66-6
sodium p-chlorobenzoate

Guidance literature:: With sodium hydroxide; at 65 ℃; Kinetics;

Reference yield:

: 14694-95-2
Wilkinson's catalyst

: 29556-29-4
N-p-Tolyl-p-chlorobenzohydroxamic acid

: [Rh(III)(triphenylphosphine)(4-ClC₆H₄C(O)N(O)C₆H₄CH₃-4')2Cl]

Guidance literature:: With Et₃N; In benzene; byproducts: 4-ClC6H4C(O)NHC6H4CH3-4', PPh3, H2O; under N2; Et3N and Rh complex successively added to soln. of ligand (molar ratio 2:1:3) in benzene; stirred for 12 h at ambient temp.; evapd. partially; filtered; filtrate evapd.; purified by thin-layer chromy. (silica gel, benzene-MeCN); yellow band sepd.; extd. with MeCN; evapd.; satisfactory elem. anal.;
DOI:10.1021/ic0106930