Diethylglyoxime

Base Information

• Chemical Name: Diethylglyoxime
• CAS No.: 4437-52-9
• Molecular Formula: C6H12N2O2
• Molecular Weight: 144.1717
• Mol file: 4437-52-9.mol

Synonyms:bipropionyl dioxime;Hexan-dioxim-(3.4);Hexane-3,4-dione dioxime;diethyl glyoxime;Hexan-3,4-dion-dioxim;diethylglyoxime;

Chemical Property of Diethylglyoxime

Chemical Property:

• Vapor Pressure: 0.0176mmHg at 25°C
• Boiling Point: 225.1°C at 760 mmHg
• Flash Point: 89.9°C
• PSA: 65.18000
• Density: 1.09g/cm³
• LogP: 1.46680

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Diethylglyoxime

There total 3 articles about Diethylglyoxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

3,4-hexanedione (4437-51-8) → diethylglyoxime (4437-52-9)

Guidance literature:

With pyridine; hydroxylamine hydrochloride; In ethanol; for 1h; Heating;

DOI:10.1021/ma0501949

Reference yield:

3,4-hexanedione (4437-51-8) → diethylglyoxime (4437-52-9)

Guidance literature:

With sodium carbonate; dann nochmals Behandeln mit Hydroxylamin-Hydrochlorid und ueberschuessigem Natriumhydroxyd;

Reference yield:

propioin (4984-85-4) → diethylglyoxime (4437-52-9)

Guidance literature:

Multi-step reaction with 2 steps

1: nitric acid

2: natrium carbonate / dann nochmals Behandeln mit Hydroxylamin-Hydrochlorid und ueberschuessigem Natriumhydroxyd

With nitric acid; sodium carbonate;

upstream raw materials:

3,4-hexanedione

propioin