1-Butanone, 1,1'-(2,4,6-trihydroxy-1,3-phenylene)bis[3-methyl-

Base Information

• Chemical Name: 1-Butanone, 1,1'-(2,4,6-trihydroxy-1,3-phenylene)bis[3-methyl-
• CAS No.: 2999-10-2
• Molecular Formula: C16H22O5
• Molecular Weight: 294.348
• Mol file: 2999-10-2.mol

Synonyms:2,4-diisovalerylphloroglucinol;2,4-isovalerylphloroglucinol;2',4',6'-Trihydroxy-3'-isovaleryl-isovalerophenon;diisovaleryl phloroglucinol;1,3-di-(3-methyl-butanoyl)-2,4,6-trihydroxybenzene;

Chemical Property of 1-Butanone, 1,1'-(2,4,6-trihydroxy-1,3-phenylene)bis[3-methyl-

Chemical Property:

• PSA: 94.83000
• LogP: 3.26100

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Butanone, 1,1'-(2,4,6-trihydroxy-1,3-phenylene)bis[3-methyl-

There total 8 articles about 1-Butanone, 1,1'-(2,4,6-trihydroxy-1,3-phenylene)bis[3-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

3,5-dihydroxyphenol (108-73-6) + isopentanoyl chloride (108-12-3) → 1,1'-(2,4,6-trihydroxy-1,3-phenylene)bis(3-methylbutan-1-one) (2999-10-2)

Guidance literature:

With treated natural zeolite mordenite; In neat (no solvent); at 20 - 80 ℃; for 0.5h; Inert atmosphere; Green chemistry;

DOI:10.1080/00397911.2019.1666282

Reference yield: 75.0%

3-methylbutyric acid (503-74-2) + 3,5-dihydroxyphenol (108-73-6) → 1,1'-(2,4,6-trihydroxy-1,3-phenylene)bis(3-methylbutan-1-one) (2999-10-2)

Guidance literature:

With boron trifluoride diethyl etherate; at 100 ℃; for 2.5h;

DOI:10.1039/c2ob25376c

Reference yield: 67.0%

3-methylbutyric acid (503-74-2) + 3,5-dihydroxyphenol (108-73-6) → phloroisovalerophenone (26103-97-9) + 1,1'-(2,4,6-trihydroxy-1,3-phenylene)bis(3-methylbutan-1-one) (2999-10-2)

Guidance literature:

With boron trifluoride diethyl etherate; at 100 ℃; for 2h;

DOI:10.1016/j.bmcl.2008.10.085

upstream raw materials:

3,5-dihydroxyphenol

isopentanoyl chloride

3-methylbutyric acid

phloroisovalerophenone

Downstream raw materials:

1,1′-(4,6-dihydroxy-5,5-dimethyl-2-oxocyclohexa-3,6-diene-1,3-diyl)bis(3-methylbutan-1-one)

C₂₀H₃₀O₅

C₂₄H₃₈O₅

C₂₄H₃₈O₅