Stannane, (1,1-dimethylethyl)triphenyl-

Base Information

Chemical Name:Stannane, (1,1-dimethylethyl)triphenyl-
CAS No.:30191-68-5
Molecular Formula:C22H24Sn
Molecular Weight:407.143
Hs Code.:
DSSTox Substance ID:DTXSID20402163
Mol file:30191-68-5.mol

Synonyms:tert-butyl(triphenyl)stannane;Stannane, (1,1-dimethylethyl)triphenyl-;30191-68-5;DTXSID20402163;AKOS024433315

Suppliers and Price of Stannane, (1,1-dimethylethyl)triphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Stannane, (1,1-dimethylethyl)triphenyl-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:408.090003
Heavy Atom Count:23
Complexity:303

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)[Sn](C1=CC=CC=C1)(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of Stannane, (1,1-dimethylethyl)triphenyl-

There total 1 articles about Stannane, (1,1-dimethylethyl)triphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.6%

: 639-58-7
triphenyltin chloride

: 30191-68-5
t-butyltriphenylstannane

Guidance literature:: With LiC(CH₃)3; In n-heptane; (C6H5)3SnCl in heptane was treated with LiC(CH3)3 in pentane at 0 .degre.C, then stirring at 25 °C for 12 h;;
DOI:10.1039/J19700002987

Reference yield: 97.0%

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 30191-68-5
t-butyltriphenylstannane

: (C₆H₅)2Sn(C(CH₃)3)I

Guidance literature:: In tetrahydrofuran; (Ar); I2 was added to soln. of Sn compd. in THF; mixt. was stirred at room temp. for 2 h;
DOI:10.1016/j.jorganchem.2006.01.023

Reference yield: 95.0%

: 227080-13-9
2-(4-bromo-phenyl)-4-isopropyl-4,5-dihydro-oxazole

: 30191-68-5
t-butyltriphenylstannane

: (R)-2-[2-(tert-butyl-diphenyl-stannyl)-phenyl]-4-isopropyl-4,5-dihydro-oxazole

Guidance literature:: With n-BuLi; I₂; In tetrahydrofuran; (Ar); I2 was added to soln. of Sn compd. in THF; mixt. was stirred at ambient temp. for 2 h; cooled to -70°C; soln. of BuLi in hexane wasadded to oxazole; obtained soln. was slowly added to Sn soln.; mixt. wa s stirred for 1 h; quenched by water; Et2O added; org. layer septd.; chromd. (silica gel plates, hexane/EtOAc); elem. anal.;
DOI:10.1016/j.jorganchem.2006.01.023