4-(N-Methyl-N-<2-(3--propionyloxy)-ethyl>-amino)-4'-nitro-azobenzol chlorid

Base Information

• Chemical Name: 4-(N-Methyl-N-<2-(3--propionyloxy)-ethyl>-amino)-4'-nitro-azobenzol chlorid
• CAS No.: 100768-79-4
• Molecular Formula: C₂₃H₃₀N₅O₅*Cl
• Molecular Weight: 491.975

Synonyms:

Chemical Property of 4-(N-Methyl-N-<2-(3--propionyloxy)-ethyl>-amino)-4'-nitro-azobenzol chlorid

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of 4-(N-Methyl-N-<2-(3--propionyloxy)-ethyl>-amino)-4'-nitro-azobenzol chlorid

There total 3 articles about 4-(N-Methyl-N-<2-(3--propionyloxy)-ethyl>-amino)-4'-nitro-azobenzol chlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitro-aniline (100-01-6,104810-17-5) → 4-(N-Methyl-N-<2-(3--propionyloxy)-ethyl>-amino)-4'-nitro-azobenzol chlorid (100768-79-4)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) (diazotization), (ii) /BRN= 6696577/, NaOAc

2: dioxane / Ambient temperature

In 1,4-dioxane;

DOI:10.1039/jr9640000883

Reference yield:

2-[(4-amino-phenyl)-methyl-amino]-ethanol → 4-(N-Methyl-N-<2-(3--propionyloxy)-ethyl>-amino)-4'-nitro-azobenzol chlorid (100768-79-4)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) (diazotization), (ii) /BRN= 6696577/, NaOAc

2: dioxane / Ambient temperature

In 1,4-dioxane;

DOI:10.1039/jr9640000883

Reference yield:

4-methyl-morpholine (109-02-4) + acryloyl chloride (814-68-6,25189-84-8) + 4'-{(2-hydroxyethyl)(methyl)amino}-4-nitroazobenzene (41616-43-7) → 4-(N-Methyl-N-<2-(3--propionyloxy)-ethyl>-amino)-4'-nitro-azobenzol chlorid (100768-79-4)

Guidance literature:

In 1,4-dioxane; Ambient temperature;

DOI:10.1039/jr9640000883

upstream raw materials:

4-methyl-morpholine

acryloyl chloride

4'-{(2-hydroxyethyl)(methyl)amino}-4-nitroazobenzene

4-nitro-aniline

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