5-phenyl-1,2,3,4-tetrathiacyclohexane

Base Information

Chemical Name:5-phenyl-1,2,3,4-tetrathiacyclohexane
CAS No.:135309-19-2
Molecular Formula:C₈H₈S₄
Molecular Weight:232.416
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-phenyl-1,2,3,4-tetrathiacyclohexane

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Technology Process of 5-phenyl-1,2,3,4-tetrathiacyclohexane

There total 1 articles about 5-phenyl-1,2,3,4-tetrathiacyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 0.5%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 10544-50-0
sulfur

: 17685-52-8
triiron dodecarbonyl

: Fe2(μ-S)2(CO)6

: Fe₂(CO)6(S₃CH₂)

: Fe₃(CO)10S

: 135309-19-2
5-phenyl-1,2,3,4-tetrathiacyclohexane

Guidance literature:: In further solvent(s); stirring of a mixt. of sulfur, Fe3(CO)12 and styrene for 15 h at 60°C under Ar to the disappearance of Fe3(CO)12 (based on TLC); cooling to 20°C, filtn., washing with hot benzene, removal of styrene and benzene in vacuo, column chromy. on silica gel (petroleum ether), elem. anal., further products;
DOI:10.1007/BF00958582

Reference yield:

: 17685-52-8
triiron dodecarbonyl

: 135309-19-2
5-phenyl-1,2,3,4-tetrathiacyclohexane

: Fe2(μ-S)2(CO)6

: Fe₂(CO)6S₂*C₆H₅CHCH₂=Fe₂(CO)6S₂(C₆H₅CHCH₂)

: Fe₃⁽⁴⁺⁾*2S^(2-)*9CO = [Fe₃S₂(CO)9]

Guidance literature:: In benzene; A mixt. of PhCHCH2S4 and Fe3(CO)12 is heated with stirring for 2.5 h at 60°C to disappearance of the polysulfide (TLC).; filtn., washing with hot benzene, solvent evapn., column chromy. on silica gel (petroleum ether), elem. anal.;
DOI:10.1007/BF00958582