5-(4-Methoxyphenyl)-3-phenyl-2-cyclohexen-1-one

Base Information

Chemical Name:5-(4-Methoxyphenyl)-3-phenyl-2-cyclohexen-1-one
CAS No.:30314-01-3
Molecular Formula:C₁₉H₁₈O₂
Molecular Weight:278.351
Hs Code.:
DSSTox Substance ID:DTXSID801241168

Synonyms:5-(4-Methoxyphenyl)-3-phenyl-2-cyclohexen-1-one;30314-01-3;DTXSID801241168

Suppliers and Price of 5-(4-Methoxyphenyl)-3-phenyl-2-cyclohexen-1-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(4-Methoxyphenyl)-3-phenyl-2-cyclohexen-1-one

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:278.130679813
Heavy Atom Count:21
Complexity:384

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C2CC(=CC(=O)C2)C3=CC=CC=C3

Technology Process of 5-(4-Methoxyphenyl)-3-phenyl-2-cyclohexen-1-one

There total 5 articles about 5-(4-Methoxyphenyl)-3-phenyl-2-cyclohexen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 3906-07-8,39212-13-0
3-(4-methoxyphenyl)-1-phenyl-2-propen-1-ol

: 123-54-6,81235-32-7
acetylacetone

: 30314-01-3
5-(4-methoxyphenyl)-3-phenyl-2-cyclohexen-1-one

Guidance literature:: 3-(4-methoxyphenyl)-1-phenyl-2-propen-1-ol; acetylacetone; With iron(III) trifluoromethanesulfonate; at 60 ℃; for 3h; Neat (no solvent);

With methanol; iron(III) trifluoromethanesulfonate; at 90 ℃; for 10h; Neat (no solvent);
DOI:10.1002/ejoc.201000128

Reference yield:

: 30313-25-8
ethyl 2-oxo-6-(4-methoxyphenyl)-4-phenyl-3-cyclohexene-1-carboxylate

: 30314-01-3
5-(4-methoxyphenyl)-3-phenyl-2-cyclohexen-1-one

Guidance literature:: With hydrogenchloride; In acetic acid;
DOI:10.1081/SCC-100104462

Reference yield:

: 22966-19-4
trans-4'-methoxychalcone

: 30314-01-3
5-(4-methoxyphenyl)-3-phenyl-2-cyclohexen-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: NaOEt

2: dil HCl / acetic acid

With hydrogenchloride; sodium ethanolate; In acetic acid; 1: Knoevenagel reaction;
DOI:10.1081/SCC-100104462