methyl (16-nitro-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)carbamate

Base Information

Chemical Name:methyl (16-nitro-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)carbamate
CAS No.:83935-77-7
Molecular Formula:C₁₆H₂₂N₂O₉
Molecular Weight:386.359
Hs Code.:

Synonyms:1,4,7,10,13-Benzopentaoxacyclopentadecin,carbamic acid deriv.; NSC 366069

Suppliers and Price of methyl (16-nitro-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of methyl (16-nitro-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)carbamate

Chemical Property:

Vapor Pressure:2.92E-10mmHg at 25°C
Boiling Point:503.4°Cat760mmHg
Flash Point:258.2°C
Density:1.277g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of methyl (16-nitro-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)carbamate

There total 6 articles about methyl (16-nitro-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin-15-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60835-69-0
4'-nitrobenzo-15-crown-5

: 83935-77-7
(3-Nitro-6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-yl)-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: H₂ / Ra-Ni / methanol; H₂O

2: 2) nitric acid / 1) glacial acetic acid, 80 deg C, 1 h, 2) 60 deg C

3: 70 percent / 18percent aq. HCl / Heating

4: 94 percent / chlorobenzene / Heating

5: CH₂Cl₂ / 2 h / Ambient temperature

With hydrogenchloride; hydrogen; nitric acid; Ra-Ni; In methanol; dichloromethane; water; chlorobenzene;

Reference yield:

: 60835-71-4
4'-aminobenzo-15-crown-5-ether

: 83935-77-7
(3-Nitro-6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-yl)-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 2) nitric acid / 1) glacial acetic acid, 80 deg C, 1 h, 2) 60 deg C

2: 70 percent / 18percent aq. HCl / Heating

3: 94 percent / chlorobenzene / Heating

4: CH₂Cl₂ / 2 h / Ambient temperature

With hydrogenchloride; nitric acid; In dichloromethane; chlorobenzene;

Reference yield:

: 77001-50-4
4'-amino-5'-nitrobenzo<15-crown-5>

: 83935-77-7
(3-Nitro-6,7,9,10,12,13,15,16-octahydro-5,8,11,14,17-pentaoxa-benzocyclopentadecen-2-yl)-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / chlorobenzene / Heating

2: CH₂Cl₂ / 2 h / Ambient temperature

In dichloromethane; chlorobenzene;