2-(2-Nitroethyl)thiophene

Base Information

Chemical Name:2-(2-Nitroethyl)thiophene
CAS No.:30807-46-6
Molecular Formula:C6H7NO2S
Molecular Weight:157.193
Hs Code.:
DSSTox Substance ID:DTXSID80455312
Nikkaji Number:J1.017.261F
Wikidata:Q82277264
Mol file:30807-46-6.mol

Synonyms:2-(2-nitroethyl)thiophene;30807-46-6;Thiophene, 2-(2-nitroethyl)-;SCHEMBL6639838;DTXSID80455312;WKCJBZNTEAWBAS-UHFFFAOYSA-N;EN300-1672419

Suppliers and Price of 2-(2-Nitroethyl)thiophene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2-(2-Nitroethyl)thiophene

Chemical Property:

PSA：74.06000
LogP:2.09050
XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:157.01974964
Heavy Atom Count:10
Complexity:123

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CSC(=C1)CC[N+](=O)[O-]

Technology Process of 2-(2-Nitroethyl)thiophene

There total 1 articles about 2-(2-Nitroethyl)thiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 874-84-0,34312-77-1
2-(2-nitroethenyl)thiophene

: 30807-46-6
2-(2-nitroethyl)thiophene

: 15509-95-2
1,3,5-tris(2-thienyl)benzene

Guidance literature:: With 1-Benzyl-1,4-dihydronicotinamide; In acetonitrile; at 80 ℃;
DOI:10.1016/S0040-4039(00)84528-1

Reference yield: 43.0%

: 30807-46-6
2-(2-nitroethyl)thiophene

: 100-52-7
benzaldehyde

: 622-79-7
benzyl azide

: 1-benzyl-5-phenyl-4-(thiophen-2-ylmethyl)-1H-1,2,3-triazole

Guidance literature:: 2-(2-nitroethyl)thiophene; benzaldehyde; With 2,6-di-tert-butyl-4-methyl-phenol; morpholinium para-toluenesulfonate; In toluene; at 100 ℃; for 1h; Sealed tube; Molecular sieve; Inert atmosphere;

benzyl azide; In toluene; at 20 - 100 ℃; for 72h; regioselective reaction; Sealed tube; Molecular sieve; Inert atmosphere;
DOI:10.1002/anie.201403453

Reference yield:

: 30807-46-6
2-(2-nitroethyl)thiophene

: 20893-30-5
2-cyanomethylthiophene

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / NaNO₂, NaOH / methanol / 0 °C

2: Et₃N / CH₂Cl₂ / Ambient temperature

3: 81 percent / Bu₃SnH, AIBN / benzene / Heating

With sodium hydroxide; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; triethylamine; sodium nitrite; In methanol; dichloromethane; benzene;
DOI:10.1016/0040-4039(96)01779-0