2-(2-{[(E)-(2-Carboxyphenyl)diazenyl](cyano)methylidene}hydrazinyl)benzoic acid

Base Information

Chemical Name:2-(2-{[(E)-(2-Carboxyphenyl)diazenyl](cyano)methylidene}hydrazinyl)benzoic acid
CAS No.:30842-82-1
Molecular Formula:C₁₆H₁₁N₅O₄
Molecular Weight:337.294
Hs Code.:
DSSTox Substance ID:DTXSID40855576
Mol file:30842-82-1.mol

Synonyms:30842-82-1;DTXSID40855576;2-(2-{[(E)-(2-Carboxyphenyl)diazenyl](cyano)methylidene}hydrazinyl)benzoic acid

Suppliers and Price of 2-(2-{[(E)-(2-Carboxyphenyl)diazenyl](cyano)methylidene}hydrazinyl)benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2-(2-{[(E)-(2-Carboxyphenyl)diazenyl](cyano)methylidene}hydrazinyl)benzoic acid

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:6
Exact Mass:337.08110385
Heavy Atom Count:25
Complexity:609

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C(=O)O)NN=C(C#N)N=NC2=CC=CC=C2C(=O)O
Isomeric SMILES:C1=CC=C(C(=C1)C(=O)O)N/N=C(\C#N)/N=NC2=CC=CC=C2C(=O)O

Technology Process of 2-(2-{[(E)-(2-Carboxyphenyl)diazenyl](cyano)methylidene}hydrazinyl)benzoic acid

There total 2 articles about 2-(2-{[(E)-(2-Carboxyphenyl)diazenyl](cyano)methylidene}hydrazinyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 65157-84-8,87429-51-4,4724-45-2
β-piperidinoacrylonitrile

: 2099-63-0,7459-95-2
anthranilic acid hydrochloride

: 30842-82-1
1,5-di(o-carboxyphenyl)-3-cyanoformazane

: 2-(N'-[1-cyano-2-oxoethylidene]hydrazino)benzoic acid

Guidance literature:: anthranilic acid hydrochloride; With hydrogenchloride; sodium nitrite; In water;

β-piperidinoacrylonitrile; With water; sodium acetate; acetic acid; at 0 - 5 ℃; for 1h;
DOI:10.1002/zaac.201600148

Reference yield:

: 17333-86-7
o-Carboxybenzenediazonium

: 1071-36-9
sodium cyanoacetate

: 30842-82-1
1,5-di(o-carboxyphenyl)-3-cyanoformazane

Guidance literature:: DOI:10.1002/hlca.19490320334

Reference yield:

: lanthanum(III) perchlorate

: 30842-82-1
1,5-di(o-carboxyphenyl)-3-cyanoformazane

: La⁽³⁺⁾*(OOCC₆H₄NNC(CN)NNC₆H₄COO)^(3-)*3H₂O*C₂H₅OH={La(OOCC₆H₄NNC(CN)NNC₆H₄COO)(H₂O)3(C₂H₅OH)}

Guidance literature:: With C₂H₅OH; In ethanol; mixing of alc. solns. of La(ClO4)3 with the requisite amt. of the formazan; elem. anal.;
DOI:10.1016/0040-6031(89)87172-2