2,5,6,6-Tetramethylcyclohex-1-ene-1-carbaldehyde

Base Information

Chemical Name:2,5,6,6-Tetramethylcyclohex-1-ene-1-carbaldehyde
CAS No.:31162-52-4
Molecular Formula:C11H18O
Molecular Weight:166.263
Hs Code.:
DSSTox Substance ID:DTXSID10560185
Nikkaji Number:J160.120B
Mol file:31162-52-4.mol

Synonyms:5-Methyl-beta-cyclocitral;31162-52-4;SCHEMBL247666;DTXSID10560185;KLDYJKVPXAEPBK-UHFFFAOYSA-N;2,5,6,6-Tetramethyl-cyclohexene carbaldehyde;2,5,6,6-tetramethyl-1-cyclohexen-1-carbaldehyde;2,5,6,6-Tetramethylcyclohex-1-ene-1-carbaldehyde

Suppliers and Price of 2,5,6,6-Tetramethylcyclohex-1-ene-1-carbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,5,6,6-Tetramethylcyclohex-1-ene-1-carbaldehyde

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:166.135765193
Heavy Atom Count:12
Complexity:223

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CCC(=C(C1(C)C)C=O)C

Technology Process of 2,5,6,6-Tetramethylcyclohex-1-ene-1-carbaldehyde

There total 10 articles about 2,5,6,6-Tetramethylcyclohex-1-ene-1-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 35906-92-4
(+/-)-α-methylcyclocitral

: 31162-52-4
2,5,6,6-tetramethylcyclohex-1-enecarbaldehyde

Guidance literature:: With potassium hydroxide; at 25 ℃; for 2h;
DOI:10.1007/BF01168096

Reference yield: 88.0%

: 31162-52-4
2,5,6,6-tetramethylcyclohex-1-enecarbaldehyde

Guidance literature:

Reference yield:

: 127348-54-3
6-phenylsulfonyl-3,6,7-trimethylocta-2E,7-dien-1-ol

: 31162-52-4
2,5,6,6-tetramethylcyclohex-1-enecarbaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: NaOEt / tetrahydrofuran / 10 °C

2: 85 percent / HSO₃F / various solvent(s) / -90 °C

3: 81 percent / CrO₃, pyridine / CH₂Cl₂ / 0.5 h / 25 °C

4: 95 percent / 8.5percent methanolic KOH / 2 h / 25 °C

With pyridine; chromium(VI) oxide; potassium hydroxide; sodium ethanolate; fluorosulphonic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1007/BF01168096