(+/-)-α-methylcyclocitral

Base Information

Chemical Name:(+/-)-α-methylcyclocitral
CAS No.:35906-92-4
Molecular Formula:C₁₁H₁₈O
Molecular Weight:166.263
Hs Code.:

Synonyms:(+/-)-α-methylcyclocitral

Suppliers and Price of (+/-)-α-methylcyclocitral

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-α-methylcyclocitral

Chemical Property:

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Technology Process of (+/-)-α-methylcyclocitral

There total 7 articles about (+/-)-α-methylcyclocitral which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 91212-46-3
α-methylcyclogeraniol

: 35906-92-4
(+/-)-α-methylcyclocitral

Guidance literature:: With pyridine; chromium(VI) oxide; In dichloromethane; at 25 ℃; for 0.5h;
DOI:10.1007/BF01168096

Reference yield:

: 35906-92-4
(+/-)-α-methylcyclocitral

Guidance literature:: With aluminum isopropoxide; at 80 - 100 ℃; under 11 Torr; anschliessend Erhitzen mit 4-Methoxy-benzaldehyd auf 130-160grad;
DOI:10.1002/hlca.19520350528

Reference yield:

: 127348-54-3
6-phenylsulfonyl-3,6,7-trimethylocta-2E,7-dien-1-ol

: 35906-92-4
(+/-)-α-methylcyclocitral

Guidance literature:: Multi-step reaction with 3 steps

1: NaOEt / tetrahydrofuran / 10 °C

2: 85 percent / HSO₃F / various solvent(s) / -90 °C

3: 81 percent / CrO₃, pyridine / CH₂Cl₂ / 0.5 h / 25 °C

With pyridine; chromium(VI) oxide; sodium ethanolate; fluorosulphonic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1007/BF01168096