(3-Methylbut-2-en-1-ylidene)(triphenyl)-lambda~5~-phosphane

Base Information

Chemical Name:(3-Methylbut-2-en-1-ylidene)(triphenyl)-lambda~5~-phosphane
CAS No.:31188-53-1
Molecular Formula:C23H23P
Molecular Weight:330.409
Hs Code.:
DSSTox Substance ID:DTXSID20526737
Mol file:31188-53-1.mol

Synonyms:31188-53-1;SCHEMBL12316043;DTXSID20526737;(3-Methylbut-2-en-1-ylidene)(triphenyl)-lambda~5~-phosphane

Suppliers and Price of (3-Methylbut-2-en-1-ylidene)(triphenyl)-lambda~5~-phosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of (3-Methylbut-2-en-1-ylidene)(triphenyl)-lambda~5~-phosphane

Chemical Property:

Boiling Point:477.8±28.0 °C(Predicted)
PSA：9.81000
Density:1.07±0.1 g/cm3(Predicted)
LogP:4.74890
XLogP3:5.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:330.153737731
Heavy Atom Count:24
Complexity:398

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CC=P(C1=CC=CC=C1)(C2=CC=CC=C2)C3=CC=CC=C3)C

Technology Process of (3-Methylbut-2-en-1-ylidene)(triphenyl)-lambda~5~-phosphane

There total 4 articles about (3-Methylbut-2-en-1-ylidene)(triphenyl)-lambda~5~-phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1530-34-3
(3-methylbut-2-enyl)triphenylphosphonium bromide

: 31188-53-1
Triphenyl-3,3-dimethyl-allylidenphosphoran

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; for 1h; Ambient temperature;
DOI:10.1021/ja981377w

Reference yield:

: 603-35-0
triphenylphosphine

: 31188-53-1
Triphenyl-3,3-dimethyl-allylidenphosphoran

Guidance literature:: Multi-step reaction with 2 steps

1: 12 h / 100 °C

2: n-butyllithium / diethyl ether; hexane / 1 h / 20 °C / Inert atmosphere

With n-butyllithium; In diethyl ether; hexane;
DOI:10.1021/ol201112a

Reference yield:

: 870-63-3
prenyl bromide

: 31188-53-1
Triphenyl-3,3-dimethyl-allylidenphosphoran

Guidance literature:: Multi-step reaction with 2 steps

1: 12 h / 100 °C

2: n-butyllithium / diethyl ether; hexane / 1 h / 20 °C / Inert atmosphere

With n-butyllithium; In diethyl ether; hexane;
DOI:10.1021/ol201112a