4-Methyl-1-phenylpent-3-en-1-one

Base Information

Chemical Name:4-Methyl-1-phenylpent-3-en-1-one
CAS No.:36597-09-8
Molecular Formula:C12H14O
Molecular Weight:174.243
Hs Code.:
DSSTox Substance ID:DTXSID30494296
Nikkaji Number:J3.473.477A
Mol file:36597-09-8.mol

Synonyms:4-methyl-1-phenylpent-3-en-1-one;36597-09-8;SCHEMBL10507643;DTXSID30494296;4-methyl-1-phenyl-3-penten-1-one

Suppliers and Price of 4-Methyl-1-phenylpent-3-en-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Methyl-1-phenylpent-3-en-1-one

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:174.104465066
Heavy Atom Count:13
Complexity:193

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=CCC(=O)C1=CC=CC=C1)C

Technology Process of 4-Methyl-1-phenylpent-3-en-1-one

There total 35 articles about 4-Methyl-1-phenylpent-3-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: C₁₂H₁₆O₂

: 36597-09-8
4-methyl-1-phenyl-3-penten-1-one

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at -78 ℃; for 0.5h; stereoselective reaction;
DOI:10.1055/s-2008-1067077

Reference yield: 96.0%

: 3017-69-4
2-methyl-1-propenylbromide

: 98-86-2
acetophenone

: 36597-09-8
4-methyl-1-phenyl-3-penten-1-one

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; lithium tert-butoxide; In tetrahydrofuran; at 22 ℃; Solvent; Temperature; regioselective reaction; Inert atmosphere;
DOI:10.1002/anie.201505895

Reference yield: 96.0%

: 25438-37-3
phenyl(trimethylsiloxy)acetonitrile

: 503-60-6
3,3-dimethyl-allyl chloride

: 36597-09-8
4-methyl-1-phenyl-3-penten-1-one

Guidance literature:: phenyl(trimethylsiloxy)acetonitrile; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

3,3-dimethyl-allyl chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 5h; Inert atmosphere;
DOI:10.1139/cjc-2013-0337