Acetyl chloride, 2,2'-[1,2-phenylenebis(oxy)]bis-

Base Information

Chemical Name:Acetyl chloride, 2,2'-[1,2-phenylenebis(oxy)]bis-
CAS No.:31250-16-5
Molecular Formula:C10H8Cl2O4
Molecular Weight:263.077
Hs Code.:
DSSTox Substance ID:DTXSID20454389
Nikkaji Number:J1.177.893C
Wikidata:Q82275888
Mol file:31250-16-5.mol

Synonyms:31250-16-5;Acetyl chloride, 2,2'-[1,2-phenylenebis(oxy)]bis-;SCHEMBL4362963;DTXSID20454389;DPOOMESCNQUGCQ-UHFFFAOYSA-N;1,2-phenylenedioxydiacetyl chloride;1,2-di-(chlorocarbonylmethoxy)-benzene;2,2'-(o-Phenylenebisoxy)bis(acetic acid chloride)

Suppliers and Price of Acetyl chloride, 2,2'-[1,2-phenylenebis(oxy)]bis-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Acetyl chloride, 2,2'-[1,2-phenylenebis(oxy)]bis-

Chemical Property:

Melting Point:48-49 °C(Solv: ligroine (8032-32-4))
Boiling Point:327.4±22.0 °C(Predicted)
PSA：52.60000
Density:1.403±0.06 g/cm3(Predicted)
LogP:1.97500
XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:261.9799641
Heavy Atom Count:16
Complexity:231

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)OCC(=O)Cl)OCC(=O)Cl

Technology Process of Acetyl chloride, 2,2'-[1,2-phenylenebis(oxy)]bis-

There total 11 articles about Acetyl chloride, 2,2'-[1,2-phenylenebis(oxy)]bis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 5411-14-3
2-[2-(2-hydroxy-2-oxoethoxy)phenoxy]acetic acid

: 31250-16-5
[2-(2-chloro-2-oxoethoxy)phenoxy]acetyl chloride

Guidance literature:: With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃; for 2h;
DOI:10.1021/acs.inorgchem.1c01274

Reference yield: 80.0%

: 31250-16-5
[2-(2-chloro-2-oxoethoxy)phenoxy]acetyl chloride

Guidance literature:

Reference yield:

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 31250-16-5
[2-(2-chloro-2-oxoethoxy)phenoxy]acetyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / aq. NaOH / 2 h / 90 °C

2: 85 percent / SOCl₂ / 4 h / 50 - 60 °C

With sodium hydroxide; thionyl chloride;
DOI:10.1055/s-2006-926357