Technology Process of (4S)-6-bromo-4-methylhexanal
There total 4 articles about (4S)-6-bromo-4-methylhexanal which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
(S)-citronellyl bromide;
With
3-chloro-benzenecarboperoxoic acid;
In
chloroform;
With
sodium periodate;
In
tetrahydrofuran; water;
DOI:10.1016/S0040-4039(00)00371-3
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: NaBH4 / methanol
2.1: Et3N
3.1: NaBr / dimethylformamide
4.1: MCPBA / CHCl3
4.2: NaIO4 / tetrahydrofuran; H2O
With
sodium tetrahydroborate; triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium bromide;
In
methanol; chloroform; N,N-dimethyl-formamide;
1.1: Reduction / 2.1: Tosylation / 3.1: Substitution / 4.1: Oxidation / 4.2: oxidative cleavage;
DOI:10.1016/S0040-4039(00)00371-3
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: Et3N
2.1: NaBr / dimethylformamide
3.1: MCPBA / CHCl3
3.2: NaIO4 / tetrahydrofuran; H2O
With
triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium bromide;
In
chloroform; N,N-dimethyl-formamide;
1.1: Tosylation / 2.1: Substitution / 3.1: Oxidation / 3.2: oxidative cleavage;
DOI:10.1016/S0040-4039(00)00371-3