Technology Process of Diborane-D 6
There total 9 articles about Diborane-D 6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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in a calibrated high vacuum line; powdered NaBD4 was added carefully to well-stirred D2SO4; crude deuteriodiborane was condensed in a trap maintained at -196°C; trap was periodically evacuated; was distilled into a bulb via a -145°C trap (isohexane/liquid nitrogen); NMR;
- Guidance literature:
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With
polyphosphoric acid;
triple vac. trap to trap distn.;
DOI:10.1063/1.437505
- Guidance literature:
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In
neat (no solvent);
calculation of react.-enthalpy and -entropy at 300K;;