Carbamic acid, (2-oxo-3-phenoxypropyl)-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, (2-oxo-3-phenoxypropyl)-, 1,1-dimethylethyl ester
CAS No.:313657-48-6
Molecular Formula:C₁₄H₁₉NO₄
Molecular Weight:265.309
Hs Code.:
DSSTox Substance ID:DTXSID40477994
Nikkaji Number:J1.483.307B
Wikidata:Q82311122
Mol file:313657-48-6.mol

Synonyms:313657-48-6;Carbamic acid, (2-oxo-3-phenoxypropyl)-, 1,1-dimethylethyl ester;SCHEMBL24096275;DTXSID40477994

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, (2-oxo-3-phenoxypropyl)-, 1,1-dimethylethyl ester

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:265.13140809
Heavy Atom Count:19
Complexity:303

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C)OC(=O)NCC(=O)COC1=CC=CC=C1

Technology Process of Carbamic acid, (2-oxo-3-phenoxypropyl)-, 1,1-dimethylethyl ester

There total 4 articles about Carbamic acid, (2-oxo-3-phenoxypropyl)-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 121282-71-1
rac-1-(N-tert-Butoxycarbonylamino)-2-hydroxy-3-phenoxypropane

: 313657-48-6
rac-1-(N-tert-Butoxycarbonylamino)-2-oxo-3-phenoxypropane

Guidance literature:: With dipyridinium dichromate; In N,N-dimethyl-formamide;
DOI:10.1039/b102895m

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 313657-48-6
rac-1-(N-tert-Butoxycarbonylamino)-2-oxo-3-phenoxypropane

Guidance literature:: Multi-step reaction with 4 steps

1: 98.1 percent / Et₃N / CH₂Cl₂

2: 88.3 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / 6 h / Heating

3: 92.2 percent / aq. KOH / 0 - 22 °C

4: 31 percent / pyridinium dichromate / dimethylformamide

With potassium hydroxide; dipyridinium dichromate; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b102895m

Reference yield:

: 78888-18-3
N-tert-butoxycarbonylprop-2-en-1-amine

: 313657-48-6
rac-1-(N-tert-Butoxycarbonylamino)-2-oxo-3-phenoxypropane

Guidance literature:: Multi-step reaction with 3 steps

1: 88.3 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / 6 h / Heating

2: 92.2 percent / aq. KOH / 0 - 22 °C

3: 31 percent / pyridinium dichromate / dimethylformamide

With potassium hydroxide; dipyridinium dichromate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b102895m