1H-Imidazole, 4-[(4-methyl-3-cyclohexen-1-yl)methyl]-, (2E)-2-butenedioate (1:1)

Base Information

Chemical Name:1H-Imidazole, 4-[(4-methyl-3-cyclohexen-1-yl)methyl]-, (2E)-2-butenedioate (1:1)
CAS No.:317338-03-7
Molecular Formula:C11H16N2.C4H4O4
Molecular Weight:292.335
Hs Code.:

Synonyms:

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Chemical Property of 1H-Imidazole, 4-[(4-methyl-3-cyclohexen-1-yl)methyl]-, (2E)-2-butenedioate (1:1)

Chemical Property:

Purity/Quality:

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Technology Process of 1H-Imidazole, 4-[(4-methyl-3-cyclohexen-1-yl)methyl]-, (2E)-2-butenedioate (1:1)

There total 8 articles about 1H-Imidazole, 4-[(4-methyl-3-cyclohexen-1-yl)methyl]-, (2E)-2-butenedioate (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 317338-02-6
C₁₁H₁₆N₂

: 317338-58-2
C₁₁H₁₆N₂

: 317338-03-7
C₄H₄O₄*C₁₁H₁₆N₂

Guidance literature:: C₁₁H₁₆N₂; C₁₁H₁₆N₂; With Celite; toluene-4-sulfonic acid; In water; 1,2-dichloro-ethane; for 20h; Heating / reflux;

With (2E)-but-2-enedioic acid;

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 317338-03-7
C₄H₄O₄*C₁₁H₁₆N₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hydride / tetrahydrofuran / 18.5 h / 0 - 20 °C

2.1: Celite; hydrogen / palladium 10% on activated carbon / ethyl acetate / 16 h

3.1: lithium aluminium tetrahydride; Celite / tetrahydrofuran / 1 h / -78 - 20 °C

4.1: oxalyl dichloride; Celite; dimethyl sulfoxide; triethylamine / dichloromethane / 2.5 h / -78 - 20 °C

5.1: Celite; sodium cyanide; dimethyl sulfoxide; triethylamine / ethanol / 5 h / 20 °C

5.2: 3.5 h / 100 °C

6.1: hydrogenchloride; Celite / acetone / 5 h

7.1: Celite; triethylamine / DMF (N,N-dimethyl-formamide) / 16 h

8.1: Celite / tetrahydrofuran / 16 h

9.1: Burgess Reagent; Celite / benzene / 1 h / 20 °C

10.1: potassium hydroxide; Celite / methanol; water / 30 h / Heating / reflux

11.1: Celite; toluene-4-sulfonic acid / water; 1,2-dichloro-ethane / 20 h / Heating / reflux

With hydrogenchloride; potassium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; Burgess Reagent; Celite; sodium cyanide; hydrogen; sodium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; acetone; benzene;

Reference yield:

: 172270-85-8
8-(methoxyformylmethylene)-1,4-dioxaspiro[4.5]decane

: 317338-03-7
C₄H₄O₄*C₁₁H₁₆N₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: Celite; hydrogen / palladium 10% on activated carbon / ethyl acetate / 16 h

2.1: lithium aluminium tetrahydride; Celite / tetrahydrofuran / 1 h / -78 - 20 °C

3.1: oxalyl dichloride; Celite; dimethyl sulfoxide; triethylamine / dichloromethane / 2.5 h / -78 - 20 °C

4.1: Celite; sodium cyanide; dimethyl sulfoxide; triethylamine / ethanol / 5 h / 20 °C

4.2: 3.5 h / 100 °C

5.1: hydrogenchloride; Celite / acetone / 5 h

6.1: Celite; triethylamine / DMF (N,N-dimethyl-formamide) / 16 h

7.1: Celite / tetrahydrofuran / 16 h

8.1: Burgess Reagent; Celite / benzene / 1 h / 20 °C

9.1: potassium hydroxide; Celite / methanol; water / 30 h / Heating / reflux

10.1: Celite; toluene-4-sulfonic acid / water; 1,2-dichloro-ethane / 20 h / Heating / reflux

With hydrogenchloride; potassium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; Burgess Reagent; Celite; sodium cyanide; hydrogen; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; acetone; benzene;