2-Allyl-2-methylcyclohexane-1,3-dione

Base Information

Chemical Name:2-Allyl-2-methylcyclohexane-1,3-dione
CAS No.:31929-07-4
Molecular Formula:C10H14O2
Molecular Weight:166.22
Hs Code.:
DSSTox Substance ID:DTXSID00472768
Nikkaji Number:J857.313A
Wikidata:Q82301903
Mol file:31929-07-4.mol

Synonyms:2-Allyl-2-methylcyclohexane-1,3-dione;31929-07-4;2-methyl-2-prop-2-enylcyclohexane-1,3-dione;2-allyl-2-methyl-1,3-cyclohexanedione;starbld0026802;1,3-Cyclohexanedione, 2-methyl-2-(2-propenyl)-;DTXSID00472768;AKOS015906958

Suppliers and Price of 2-Allyl-2-methylcyclohexane-1,3-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2-Allyl-2-methylcyclohexane-1,3-dione

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:166.099379685
Heavy Atom Count:12
Complexity:212

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(C(=O)CCCC1=O)CC=C

Technology Process of 2-Allyl-2-methylcyclohexane-1,3-dione

There total 10 articles about 2-Allyl-2-methylcyclohexane-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1193-55-1
2-methylcyclohexane-1,3-dione

: 107-18-6
allyl alcohol

: 31929-07-4
2-allyl-2-methyl-1,3-cyclohexanedione

Guidance literature:: With [RuCp(η³-C₃H₅)(QA)]PF_6,QA=quinaldic acid; In dichloromethane; at 80 ℃; for 5h; Inert atmosphere; Sealed tube;

Reference yield: 89.0%

: 1193-55-1
2-methylcyclohexane-1,3-dione

: 106-95-6
allyl bromide

: 31929-07-4
2-allyl-2-methyl-1,3-cyclohexanedione

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 40 ℃;
DOI:10.3998/ark.5550190.0012.229

Reference yield: 81.0%

: 1193-55-1
2-methylcyclohexane-1,3-dione

: 100-44-7
benzyl chloride

: 31929-06-3
3-Allyloxy-2-methyl-2-cyclohexen-1-on

: 31929-07-4
2-allyl-2-methyl-1,3-cyclohexanedione

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium bromide; In tetrahydrofuran; 1.) 30 min, r.t.; 2.) 11 h, ref.;
DOI:10.1055/s-1995-4064