Benzoic acid, 4-methoxy-, (1R,6R)-6-hydroxy-4-[[(4R,6S)-6-[(2S)-4-hydroxy-2-[(4-methoxybenzoyl) oxy]butyl]-2,2-dimethyl-1,3-dioxan-4-yl]methyl]-3-cyclohepten-1-yl ester

Base Information

Chemical Name:Benzoic acid, 4-methoxy-, (1R,6R)-6-hydroxy-4-[[(4R,6S)-6-[(2S)-4-hydroxy-2-[(4-methoxybenzoyl) oxy]butyl]-2,2-dimethyl-1,3-dioxan-4-yl]methyl]-3-cyclohepten-1-yl ester
CAS No.:321146-37-6
Molecular Formula:C34H44O10
Molecular Weight:612.717
Hs Code.:

Benzoic acid, 4-methoxy-,
(1R,6R)-6-hydroxy-4-[[(4R,6S)-6-[(2S)-4-hydroxy-2-[(4-methoxybenzoyl)
oxy]butyl]-2,2-dimethyl-1,3-dioxan-4-yl]methyl]-3-cyclohepten-1-yl ester

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Chemical Property of Benzoic acid, 4-methoxy-, (1R,6R)-6-hydroxy-4-[[(4R,6S)-6-[(2S)-4-hydroxy-2-[(4-methoxybenzoyl) oxy]butyl]-2,2-dimethyl-1,3-dioxan-4-yl]methyl]-3-cyclohepten-1-yl ester

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MSDS Files:: SDS file from LookChem

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Technology Process of Benzoic acid, 4-methoxy-, (1R,6R)-6-hydroxy-4-[[(4R,6S)-6-[(2S)-4-hydroxy-2-[(4-methoxybenzoyl) oxy]butyl]-2,2-dimethyl-1,3-dioxan-4-yl]methyl]-3-cyclohepten-1-yl ester

There total 2 articles about Benzoic acid, 4-methoxy-, (1R,6R)-6-hydroxy-4-[[(4R,6S)-6-[(2S)-4-hydroxy-2-[(4-methoxybenzoyl) oxy]butyl]-2,2-dimethyl-1,3-dioxan-4-yl]methyl]-3-cyclohepten-1-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 77-76-9
2,2-dimethoxy-propane

: 321146-33-2
(1R,6R)-6-Hydroxy-4-{(2R,4S,6S)-2,4,8-trihydroxy-6-[(4-methoxybenzoyl)oxy]octyl}cyclohept-1-en-1-yl 4-methoxybenzoate

: 321146-37-6
(-)-(1R,6R)-6-hydroxy-4-[[(4R,6S)-6-[(2S)-4-hydroxy-2-[(4-methoxybenzoyl)oxy]butyl]-2,2-dimethyl-1,3-dioxan-4-yl]methyl]cyclohept-3-en-1-yl 4-methoxybenzoate

Guidance literature:: With pyridinium p-toluenesulfonate; In acetone; at 0 ℃; for 4h;
DOI:10.1021/jo010172u

Reference yield:

: (2RS,4S,6R)-Tetrahydro-2-hydroxy-6-{(4S,6S)-{6-hydroxy-4-[(4-methoxybenzoyl)oxy]cyclohept-1-en-1-yl}-2-oxopropyl}-2H-pyrann-4-yl 4-methoxybenzoate

: 321146-37-6
(-)-(1R,6R)-6-hydroxy-4-[[(4R,6S)-6-[(2S)-4-hydroxy-2-[(4-methoxybenzoyl)oxy]butyl]-2,2-dimethyl-1,3-dioxan-4-yl]methyl]cyclohept-3-en-1-yl 4-methoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / Me₄NBH(OAc)3 / acetic acid / 15 h / 20 °C

2: 84 percent / pyridinium para-toluenesulfonate / acetone / 4 h / 0 °C

With pyridinium p-toluenesulfonate; tetramethylammonium triacetoxyborohydride; In acetic acid; acetone;
DOI:10.1002/1521-3765(20001117)6:22<4091::AID-CHEM4091>3.0.CO;2-W