chloro(ethyl)bis(2,4,6-trimethylphenyl)germanium

Base Information

• Chemical Name: chloro(ethyl)bis(2,4,6-trimethylphenyl)germanium
• CAS No.: 1239426-11-9
• Molecular Formula: C₂₀H₂₇ClGe
• Molecular Weight: 375.477
• Mol file: 1239426-11-9.mol

Synonyms:

Chemical Property of chloro(ethyl)bis(2,4,6-trimethylphenyl)germanium

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of chloro(ethyl)bis(2,4,6-trimethylphenyl)germanium

There total 1 articles about chloro(ethyl)bis(2,4,6-trimethylphenyl)germanium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

chloroform-d1 (865-49-6) + ([(i-Pr)2C3N2Me2]Ge(2,4,6-trimethylphenyl)2Et)I (1239426-13-1) → chloro(ethyl)bis(2,4,6-trimethylphenyl)germanium (1239426-11-9)

Guidance literature:

In chloroform-d1; (N2), Schlenk techniques; soln. of Ge compd. in CDCl3 stored for 10 min; extn. with satd. soln. of NH4Cl, aq. phase washed with CH2Cl2, combined org. phases dried over MgSO4, filtration, filtrate evapd., residue dissolved in hexanes, filtration through silica, evapn.;

DOI:10.1021/om100059z

upstream raw materials:

chloroform-d1

([(i-Pr)2C₃N₂Me₂]Ge(2,4,6-trimethylphenyl)2Et)I