2-[(2,4-DICHLOROBENZYL)OXY]-1-NAPHTHALDEHYDE

Base Information

• Chemical Name: 2-[(2,4-DICHLOROBENZYL)OXY]-1-NAPHTHALDEHYDE
• CAS No.: 321432-08-0
• Molecular Formula: C18H12Cl2O2
• Molecular Weight: 331.19
• Mol file: 321432-08-0.mol

Synonyms:

Chemical Property of 2-[(2,4-DICHLOROBENZYL)OXY]-1-NAPHTHALDEHYDE

Chemical Property:

• Melting Point: 178-180°C

Purity/Quality:

98%min ^*data from raw suppliers

2-[(2,4-Dichlorobenzyl)oxy]-1-naphthaldehyde >95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-[(2,4-DICHLOROBENZYL)OXY]-1-NAPHTHALDEHYDE

There total 1 articles about 2-[(2,4-DICHLOROBENZYL)OXY]-1-NAPHTHALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2,4-Dichlorobenzyl chloride (94-99-5) + 2-hydroxynaphthalene-1-carbaldehyde (708-06-5) → 2-((2,4-dichlorobenzyl)oxy)-1-naphthaldehyde (321432-08-0)

Guidance literature:

2-hydroxynaphthalene-1-carbaldehyde; With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 1h;

2,4-Dichlorobenzyl chloride; In N,N-dimethyl-formamide; at 60 ℃; for 2.5h;

DOI:10.1016/j.ejmech.2022.114196

Reference yield: 61.0%

2-((2,4-dichlorobenzyl)oxy)-1-naphthaldehyde (321432-08-0) + ethanolamine (141-43-5) → 2-(((2-((2,4-dichlorobenzyl)oxy)naphthalen-1-yl)methyl)amino)ethan-1-ol (774191-94-5)

Guidance literature:

2-((2,4-dichlorobenzyl)oxy)-1-naphthaldehyde; monoethanolamine; With acetic acid; In methanol; at 20 ℃; for 2h;

With sodium tris(acetoxy)borohydride; In methanol; for 10h;

DOI:10.1016/j.ejmech.2022.114196

upstream raw materials:

2,4-Dichlorobenzyl chloride

2-hydroxynaphthalene-1-carbaldehyde

Downstream raw materials:

2-(((2-((2,4-dichlorobenzyl)oxy)naphthalen-1-yl)methyl)amino)ethan-1-ol

Refernces