Dimethyl 3,4,5,6-tetrapropylbenzene-1,2-dicarboxylate

Base Information

Chemical Name:Dimethyl 3,4,5,6-tetrapropylbenzene-1,2-dicarboxylate
CAS No.:323583-96-6
Molecular Formula:C22H34O4
Molecular Weight:362.51
Hs Code.:
DSSTox Substance ID:DTXSID80573186
Nikkaji Number:J1.491.183I
Wikidata:Q82461793

Synonyms:323583-96-6;Dimethyl 3,4,5,6-tetrapropylbenzene-1,2-dicarboxylate;DTXSID80573186;AOOXGIOUJGNDEN-UHFFFAOYSA-N;Dimethyl 3,4,5,6-tetrapropylphthalate

Suppliers and Price of Dimethyl 3,4,5,6-tetrapropylbenzene-1,2-dicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Dimethyl 3,4,5,6-tetrapropylbenzene-1,2-dicarboxylate

Chemical Property:

XLogP3:7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:12
Exact Mass:362.24570956
Heavy Atom Count:26
Complexity:394

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC1=C(C(=C(C(=C1CCC)C(=O)OC)C(=O)OC)CCC)CCC

Technology Process of Dimethyl 3,4,5,6-tetrapropylbenzene-1,2-dicarboxylate

There total 4 articles about Dimethyl 3,4,5,6-tetrapropylbenzene-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 762-42-5
dimethyl acetylenedicarboxylate

: (4Z,6Z)-5,6-dipropyl-4,7-diiododeca-4,6-diene

: 323583-96-6
dimethyl 3,4,5,6-tetrapropylbenzene-1,2-dicarboxylate

Guidance literature:: (4Z,6Z)-5,6-dipropyl-4,7-diiododeca-4,6-diene; With n-butyllithium; In diethyl ether; at -78 ℃; for 1h;

With aluminium trichloride; In diethyl ether; at 20 ℃; for 1h;

dimethyl acetylenedicarboxylate; In diethyl ether; at -78 - 20 ℃;
DOI:10.1016/S0040-4020(03)00522-2

Reference yield:

: 1942-45-6
4-Octyne

: 762-42-5
dimethyl acetylenedicarboxylate

: 323583-96-6
dimethyl 3,4,5,6-tetrapropylbenzene-1,2-dicarboxylate

Guidance literature:: 4-Octyne; dipropylzirconocene; In tetrahydrofuran; at -78 - 20 ℃; for 1h;

dimethyl acetylenedicarboxylate; With copper(l) chloride; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield:

: 1942-45-6
4-Octyne

: 762-42-5
dimethyl acetylenedicarboxylate

: 323583-96-6
dimethyl 3,4,5,6-tetrapropylbenzene-1,2-dicarboxylate

: 3,4-Dibutyl-5,6-dipropyl-phthalic acid dimethyl ester

Guidance literature:: With dibutylbis(cyclopentadienyl)zirconium; ethene; hex-3-yne; copper(l) chloride; Yield given. Multistep reaction. Yields of byproduct given;
DOI:10.1021/ja970869q