Methanone, (4-chlorophenyl)(2,4,6-trimethylphenyl)-

Base Information

Chemical Name:Methanone, (4-chlorophenyl)(2,4,6-trimethylphenyl)-
CAS No.:32363-44-3
Molecular Formula:C16H15ClO
Molecular Weight:258.748
Hs Code.:2914700090
DSSTox Substance ID:DTXSID00455516
Nikkaji Number:J617.322E
Mol file:32363-44-3.mol

Synonyms:32363-44-3;(4-chlorophenyl)(mesityl)methanone;Methanone, (4-chlorophenyl)(2,4,6-trimethylphenyl)-;2,4,6-Trimethyl-4'-chlorobenzophenone;4-chlorobenzoylmesitylene;SCHEMBL7264522;DTXSID00455516;WPNFQDQJGMMQPU-UHFFFAOYSA-N

Suppliers and Price of Methanone, (4-chlorophenyl)(2,4,6-trimethylphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Methanone, (4-chlorophenyl)(2,4,6-trimethylphenyl)-

Chemical Property:

Melting Point:68-69.5 °C
Boiling Point:178 °C(Press: 5 Torr)
PSA：17.07000
Density:1.133±0.06 g/cm3(Predicted)
LogP:4.49620
XLogP3:5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:258.0811428
Heavy Atom Count:18
Complexity:282

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C(=C1)C)C(=O)C2=CC=C(C=C2)Cl)C

Technology Process of Methanone, (4-chlorophenyl)(2,4,6-trimethylphenyl)-

There total 7 articles about Methanone, (4-chlorophenyl)(2,4,6-trimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 122-01-0
4-chloro-benzoyl chloride

: 108-67-8
1,3,5-trimethyl-benzene

: 32363-44-3
(4-chlorophenyl)-(2,4,6-trimethylphenyl)methanone

Guidance literature:: With C₄F₉SO₃H; at 165 ℃; for 2h;

Reference yield: 81.0%

: 1126-46-1
Methyl 4-chlorobenzoate

: 108-67-8
1,3,5-trimethyl-benzene

: 32363-44-3
(4-chlorophenyl)-(2,4,6-trimethylphenyl)methanone

Guidance literature:: With iodine; phosphorus trichloride; In acetonitrile; at 160 ℃; Sealed tube; Schlenk technique;
DOI:10.1021/acs.joc.0c02794

Reference yield: 70.0%

: 576-83-0
2,4,6-trimethylphenyl bromide

: 104-88-1
4-chlorobenzaldehyde

: 32363-44-3
(4-chlorophenyl)-(2,4,6-trimethylphenyl)methanone

Guidance literature:: 2,4,6-trimethylphenyl bromide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

4-chlorobenzaldehyde; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1h;

With iodine; potassium carbonate; In tert-butyl alcohol; for 18h; Reflux;
DOI:10.1016/j.tet.2011.12.023