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Para Chloro Benzoyl Chloride, 4-Chlorobenzoyl chloride, PCBC, Rebamipide raw meterial
Cas No: 122-01-0
No Data 1 Kilogram 1 Kilogram/Day hangzhou verychem science and technology co.ltd Contact Supplier
4-Chlorobenzoyl chloride 122-01-0
Cas No: 122-01-0
No Data No Data No Data Hunan Russell Chemicals Technology Co.,Ltd Contact Supplier
4-Chlorobenzoyl chloride
Cas No: 122-01-0
USD $ 10.0-10.0 / Kilogram 1000 Kilogram 100 Metric Ton/Month Quzhou Hopemax Chemical Technology Co.Ltd Contact Supplier
4-Chlorobenzoyl chloride -Low Price High Quality
Cas No: 122-01-0
No Data 1 Kilogram 2 Metric Ton/Day Nantong Leadchem Industry Co.,Ltd Contact Supplier
4-Chlorobenzoyl chloride
Cas No: 122-01-0
No Data No Data No Data Pure Chemistry Scientific Inc. Contact Supplier

122-01-0 Usage

Chemical Properties

liquid

Definition

ChEBI: An acyl chloride consisting of benzoyl chloride having a chloro substituent in the para-position.

Uses

4-Chlorobenzoyl Chloride is used as a promoter in the synthesis of α-aminonitriles. It is also used as a derivatization agent and self-assembling dipole molecule to improve hole injection in conjugated polymers. In addition. It is an important organic intermediate to synthetize substituted 4-chlorobenzoyl products.
InChI:InChI:1S/C7H4Cl2O/c8-6-3-1-5(2-4-6)7(9)10/h1-4H

122-01-0 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Alfa Aesar (A16325)  4-Chlorobenzoyl chloride, 98%    122-01-0 25g 175.0CNY Detail
Alfa Aesar (A16325)  4-Chlorobenzoyl chloride, 98%    122-01-0 100g 253.0CNY Detail
Alfa Aesar (A16325)  4-Chlorobenzoyl chloride, 98%    122-01-0 500g 567.0CNY Detail
Aldrich (111902)  4-Chlorobenzoylchloride  99% 122-01-0 111902-5G 394.29CNY Detail
Aldrich (111902)  4-Chlorobenzoylchloride  99% 122-01-0 111902-100G 370.89CNY Detail
Aldrich (111902)  4-Chlorobenzoylchloride  99% 122-01-0 111902-500G 1,490.58CNY Detail
Aldrich (374288)  4-Chlorobenzoylchloride  95% 122-01-0 374288-25ML 503.10CNY Detail
Aldrich (374288)  4-Chlorobenzoylchloride  95% 122-01-0 374288-2L 2,652.39CNY Detail

122-01-0SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name 4-chlorobenzoyl chloride

1.2 Other means of identification

Product number -
Other names p-Chlorobenzoly chloride

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:122-01-0 SDS

122-01-0Synthetic route

para-chlorobenzoic acid
74-11-3

para-chlorobenzoic acid

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃;100%
With thionyl chloride for 2h; Reflux;100%
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 2h; Reflux;100%
3-chlorophthalic anhydride
117-21-5

3-chlorophthalic anhydride

4-chlorotrichloromethylbenzene
5216-25-1

4-chlorotrichloromethylbenzene

A

3-chloro-phthaloyl dichloride
113770-84-6

3-chloro-phthaloyl dichloride

B

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
zirconium(IV) chloride at 160℃; for 16h;A 61%
B 95%
phthalic anhydride
85-44-9

phthalic anhydride

4-chlorotrichloromethylbenzene
5216-25-1

4-chlorotrichloromethylbenzene

A

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

B

Phthaloyl dichloride
88-95-9

Phthaloyl dichloride

Conditions
ConditionsYield
zirconium(IV) chloride at 160℃; for 6h;A 93%
B 70%
1-Chloro-4-iodobenzene
637-87-6

1-Chloro-4-iodobenzene

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

A

p-nitrobenzene iodide
636-98-6

p-nitrobenzene iodide

B

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 90℃; for 20h; Sealed tube; Inert atmosphere;A n/a
B 93%
tert-butyl 4-chlorobenzoate
712-95-8

tert-butyl 4-chlorobenzoate

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
With phosphorus trichloride In acetonitrile at 80℃; for 3h; Schlenk technique;89%
oxalyl dichloride
79-37-8

oxalyl dichloride

chlorobenzene
108-90-7

chlorobenzene

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
Stage #1: oxalyl dichloride With aluminum (III) chloride In dichloromethane for 0.0833333h;
Stage #2: chlorobenzene In dichloromethane at 20 - 25℃; for 1h;
77.7%
With aluminium trichloride; lithium perchlorate In nitromethane at 20℃; for 10h;
With aluminium trichloride In dichloromethane at 20℃; for 14h; chlorocarbonylation; Friedel-Crafts reaction;
para-chlorotoluene
106-43-4

para-chlorotoluene

A

4-chlorobenzaldehyde
104-88-1

4-chlorobenzaldehyde

B

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
With dioxochloro(trimethylsiloxy)chromate(VI) In 1,2-dichloro-ethane for 4.5h; Heating; Yields of byproduct given;A 55%
B n/a
Cyclopentanecarboxylic acid chloride
4524-93-0

Cyclopentanecarboxylic acid chloride

1-(pyridin-2-ylethynyl)-3-azabicyclo[3.1.0]hexane

1-(pyridin-2-ylethynyl)-3-azabicyclo[3.1.0]hexane

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
Stage #1: 1-(pyridin-2-ylethynyl)-3-azabicyclo[3.1.0]hexane With triethylamine In tetrahydrofuran; N,N-dimethyl-formamide at 0℃; for 0.166667h;
Stage #2: Cyclopentanecarboxylic acid chloride In tetrahydrofuran; N,N-dimethyl-formamide at 0 - 25℃; for 2h;
18%
benzoyl chloride
98-88-4

benzoyl chloride

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
With chlorine; iron(III) chloride at 35℃;
acetic acid
64-19-7

acetic acid

chlorobenzene
108-90-7

chlorobenzene

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
With tetrachloromethane; tungsten(IV) oxide
With tetrachloromethane; tungsten(IV) oxide
p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
With thionyl chloride at 240℃;
1-(p-chlorobenzoyl)-3-methylimidazolium chloride
93342-80-4

1-(p-chlorobenzoyl)-3-methylimidazolium chloride

A

1-methyl-1H-imidazole
616-47-7

1-methyl-1H-imidazole

B

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
In dichloromethane at 25℃; Rate constant; Equilibrium constant;
4-chloro-trichloromethyl-benzene

4-chloro-trichloromethyl-benzene

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
With water; iron(III) chloride at 100 - 120℃;
oxalyl dichloride
79-37-8

oxalyl dichloride

sodium-4-chloro benzoate

sodium-4-chloro benzoate

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
With benzene
oxalyl dichloride
79-37-8

oxalyl dichloride

sodium-<4-chloro benzoate>

sodium-<4-chloro benzoate>

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
With Petroleum ether
1-methyl-4-nitrobenzene
99-99-0

1-methyl-4-nitrobenzene

phosphorus pentachloride
10026-13-8, 874483-75-7

phosphorus pentachloride

A

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

B

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
at 180℃; Einleiten von Chlor;
1-methyl-4-nitrobenzene
99-99-0

1-methyl-4-nitrobenzene

P2O5

P2O5

A

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

B

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

Conditions
ConditionsYield
at 180℃; Einleiten von Chlor;
phosphorus pentachloride
10026-13-8, 874483-75-7

phosphorus pentachloride

4-dichlorophosphoryl-benzoyl chloride
40578-28-7

4-dichlorophosphoryl-benzoyl chloride

A

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

C

phosphorus trichloride
7719-12-2, 52843-90-0

phosphorus trichloride

Conditions
ConditionsYield
at 200℃;
phosphorus pentachloride
10026-13-8, 874483-75-7

phosphorus pentachloride

4-dichlorophosphoryloxy-benzoyl chloride
20070-01-3

4-dichlorophosphoryloxy-benzoyl chloride

A

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

B

4-chloro-trichloromethyl-benzene

4-chloro-trichloromethyl-benzene

Conditions
ConditionsYield
at 170 - 180℃;
para-chlorotoluene
106-43-4

para-chlorotoluene

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: diluted permanganate
2: PCl5
View Scheme
Multi-step reaction with 2 steps
1: chlorine / 80 - 180 °C / Irradiation
2: iron(III) chloride; para-chlorobenzoic acid / melt / 100 - 110 °C
View Scheme
methyl 5-(4-aminobenzyl)-1-(4-tert-butoxycarbonylaminomethylphenyl)-2,4-dioxo-2,3,4,5-tetrahydro-1H-1,5-benzodiazepine-3-acetate
264915-91-5

methyl 5-(4-aminobenzyl)-1-(4-tert-butoxycarbonylaminomethylphenyl)-2,4-dioxo-2,3,4,5-tetrahydro-1H-1,5-benzodiazepine-3-acetate

A

N-(2-fluorobenzyl)-1-(4-aminomethylphenyl)-5-[4-(4-chlorobenzoylamino)benzyl]-2,4-dioxo-2,3,4,5-tetrahydro-1H-1,5-benzodiazepine-3-acetamide hydrochloride
264915-33-5

N-(2-fluorobenzyl)-1-(4-aminomethylphenyl)-5-[4-(4-chlorobenzoylamino)benzyl]-2,4-dioxo-2,3,4,5-tetrahydro-1H-1,5-benzodiazepine-3-acetamide hydrochloride

B

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

4-chlorotrichloromethylbenzene
5216-25-1

4-chlorotrichloromethylbenzene

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
With FeCl3 In water
With sulfuric acid; acetic anhydride
With iron(III) chloride; para-chlorobenzoic acid In melt at 100 - 110℃;
1-chloro-4-trifluoromethyl-cyclohex-1-ene

1-chloro-4-trifluoromethyl-cyclohex-1-ene

4-chloro-cyclohex-3-enecarbonyl chloride
133058-06-7

4-chloro-cyclohex-3-enecarbonyl chloride

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
With bromine
4-chlorotrichloromethylbenzene
5216-25-1

4-chlorotrichloromethylbenzene

iron(II) sulfate

iron(II) sulfate

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
In water
FeCl3(«20/6,5 » mmol)

FeCl3(«20/6,5 » mmol)

4-chlorotrichloromethylbenzene
5216-25-1

4-chlorotrichloromethylbenzene

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
In water
2-(4,5-Dihydro-1,3-oxazol-2-yl)aniline
3416-93-1

2-(4,5-Dihydro-1,3-oxazol-2-yl)aniline

para-chlorobenzoic acid
74-11-3

para-chlorobenzoic acid

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
With oxalyl dichloride In dichloromethane; N,N-dimethyl-formamide
4-chlorobenzaldehyde
104-88-1

4-chlorobenzaldehyde

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
With trichloroisocyanuric acid In dichloromethane at 20℃; for 120h; Inert atmosphere;
With tert.-butylhydroperoxide; N-chloro-succinimide; tris(2,2'-bipyridyl)ruthenium dichloride In acetonitrile at 20℃; for 24h; Sealed tube; Irradiation;
With trichloroisocyanuric acid In dichloromethane at 20℃; Inert atmosphere;
para-Chlorobenzyl alcohol
873-76-7

para-Chlorobenzyl alcohol

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

Conditions
ConditionsYield
With trichloroisocyanuric acid In dichloromethane at 20℃; for 120h; Inert atmosphere;
With trichloroisocyanuric acid In dichloromethane at 20℃; Inert atmosphere;
With trichloroisocyanuric acid In dichloromethane at 20℃; Inert atmosphere;
4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

anthranilic acid
118-92-3

anthranilic acid

N-(4-chlorobenzoyl)anthranilic acid
34425-87-1

N-(4-chlorobenzoyl)anthranilic acid

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 20℃;100%
With triethylamine In dichloromethane at 0℃;95%
With sodium hydroxide
4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

diethylamine
109-89-7

diethylamine

4-chloro-N,N-diethyl-benzamide
7461-38-3

4-chloro-N,N-diethyl-benzamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 6h;100%
With sodium carbonate In tert-butyl methyl ether; water at 15 - 25℃; for 1h; Schotten-Baumann Reaction; Inert atmosphere;98.7%
In toluene at 50℃;90%
4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

phenylhydrazine
100-63-0

phenylhydrazine

2-(4-Chlorbenzoyl)-1-phenylhydrazid
15089-07-3

2-(4-Chlorbenzoyl)-1-phenylhydrazid

Conditions
ConditionsYield
With pyridine In tetrahydrofuran at 5 - 20℃; for 2h;100%
With pyridine for 20h;70%
With pyridine
silver trifluoromethanesulfonate
2923-28-6

silver trifluoromethanesulfonate

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

4-Chlorbenzoesaeure-trifluormethansulfonsaeure-anhydrid
36967-87-0

4-Chlorbenzoesaeure-trifluormethansulfonsaeure-anhydrid

Conditions
ConditionsYield
100%
at 20℃; for 3h;90%
isobutylamine
78-81-9

isobutylamine

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

4-Chloro-N-isobutyl-benzamid
7461-33-8

4-Chloro-N-isobutyl-benzamid

Conditions
ConditionsYield
With triethylamine In benzene100%
N-phenylsulfonylpyrrole
16851-82-4

N-phenylsulfonylpyrrole

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

(1-benzenesulfonyl-1H-pyrrol-3-yl)-(4-chlorophenyl)methanone
97188-31-3

(1-benzenesulfonyl-1H-pyrrol-3-yl)-(4-chlorophenyl)methanone

Conditions
ConditionsYield
With aluminium trichloride In dichloromethane for 0.5h; Ambient temperature;100%
Stage #1: 4-chloro-benzoyl chloride With aluminum (III) chloride In 1,2-dichloro-ethane at 25℃; for 0.166667h; Inert atmosphere;
Stage #2: N-phenylsulfonylpyrrole In 1,2-dichloro-ethane at 25℃; for 5h; Inert atmosphere; regioselective reaction;
100%
With aluminium trichloride In 1,2-dichloro-ethane at 25℃; for 1.5h;89%
4-Aminobutanol
13325-10-5

4-Aminobutanol

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

4-chloro-N-(4-hydroxybutyl)benzamide
130340-60-2

4-chloro-N-(4-hydroxybutyl)benzamide

Conditions
ConditionsYield
With sodium hydroxide In chloroform; water for 0.75h; Cooling with ice;100%
Stage #1: 4-chloro-benzoyl chloride With pyridine; Merrifield's resin-bound 6-methyl-2-thiouracil In dichloromethane at 80℃; for 0.0833333h; microwave irradiation;
Stage #2: 4-Aminobutanol In dichloromethane at 80℃; for 0.0833333h; microwave irradiation;
70%
With triethylamine at 0℃;
2-(4-aminophenoxy)-2-methyl propionic acid
117011-70-8

2-(4-aminophenoxy)-2-methyl propionic acid

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

2-<4-(4-chlorobenzamido)phenoxy>-2-methylpropionic acid
121809-58-3

2-<4-(4-chlorobenzamido)phenoxy>-2-methylpropionic acid

Conditions
ConditionsYield
With pyridine at 0℃;100%
With sodium hydroxide In tetrahydrofuran for 1h;90%
2-aminoacetophenone hydrochloride
5468-37-1

2-aminoacetophenone hydrochloride

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

4-Chloro-N-[1-(2-oxo-2-phenylethyl)]benzamide
82221-13-4

4-Chloro-N-[1-(2-oxo-2-phenylethyl)]benzamide

Conditions
ConditionsYield
With sodium hydrogencarbonate In ethyl acetate Ambient temperature;100%
With pyridine Acylation; Heating;78.5%
With sodium acetate for 4h;42%
ammonium thiocyanate
1147550-11-5

ammonium thiocyanate

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

p-chlorobenzoyl isothiocyanate
16794-67-5

p-chlorobenzoyl isothiocyanate

Conditions
ConditionsYield
With PEG-400 In ethyl acetate at 20℃;100%
In acetone for 1h; Heating;
In acetone
2,3,4,6-tetra-O-acetyl-5-thio-D-glucopyranose
137886-82-9

2,3,4,6-tetra-O-acetyl-5-thio-D-glucopyranose

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

2,3,4,6-tetra-O-acetyl-1-O-(4-chlorophenyl)-5-thio-α-D-glucopyranose

2,3,4,6-tetra-O-acetyl-1-O-(4-chlorophenyl)-5-thio-α-D-glucopyranose

Conditions
ConditionsYield
With pyridine for 2h; Ambient temperature;100%
2-ethoxycarbonyethylzinc iodide
104089-16-9

2-ethoxycarbonyethylzinc iodide

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

ethyl 4-(4-chlorophenyl)-4-oxobutanoate
53503-49-4

ethyl 4-(4-chlorophenyl)-4-oxobutanoate

Conditions
ConditionsYield
tetrakis(triphenylphosphine) palladium(0) In N,N-dimethyl acetamide; benzene at 60℃; for 0.5h; various co-solvents;100%
tetrakis(triphenylphosphine) palladium(0) In N,N-dimethyl acetamide; benzene at 60℃; for 0.5h;100%
4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

1-(2-oxazolinyl)indole
140934-56-1

1-(2-oxazolinyl)indole

4-Chloro-N-(2-chloro-ethyl)-N-(indole-1-carbonyl)-benzamide

4-Chloro-N-(2-chloro-ethyl)-N-(indole-1-carbonyl)-benzamide

Conditions
ConditionsYield
In benzene for 12h; Heating;100%
4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

2-methoxy-4,4,5,5-tetramethyl-1,3,2-dioxaphospholane
14812-60-3

2-methoxy-4,4,5,5-tetramethyl-1,3,2-dioxaphospholane

(4-Chloro-phenyl)-(4,4,5,5-tetramethyl-2-oxo-2λ5-[1,3,2]dioxaphospholan-2-yl)-methanone
108429-38-5

(4-Chloro-phenyl)-(4,4,5,5-tetramethyl-2-oxo-2λ5-[1,3,2]dioxaphospholan-2-yl)-methanone

Conditions
ConditionsYield
at 0℃;100%
4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

N-[(thien-3-ylcarbonyl)methyl]amine hydrochloride
85210-58-8

N-[(thien-3-ylcarbonyl)methyl]amine hydrochloride

N-(4-chlorobenzoyl)aminomethyl(3-thienyl)ketone
85210-63-5

N-(4-chlorobenzoyl)aminomethyl(3-thienyl)ketone

Conditions
ConditionsYield
With sodium hydrogencarbonate In ethyl acetate Ambient temperature;100%
With sodium hydrogencarbonate
4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

aminomethyl 3-furyl ketone hydrochloride
88352-90-3

aminomethyl 3-furyl ketone hydrochloride

N-<(4-chlorobenzoyl)amino>methyl 3-furyl ketone
88352-91-4

N-<(4-chlorobenzoyl)amino>methyl 3-furyl ketone

Conditions
ConditionsYield
With sodium hydrogencarbonate100%
With sodium hydrogencarbonate In water; ethyl acetate Ambient temperature; Yield given;
4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

4-chloro-N-hydroxybenzamide
1613-88-3

4-chloro-N-hydroxybenzamide

Conditions
ConditionsYield
With hydroxylamine hydrochloride; sodium hydrogencarbonate In water; ethyl acetate at 20℃; for 0.0833333h;100%
With hydroxylamine hydrochloride; sodium hydrogencarbonate In water; ethyl acetate at 20℃; for 0.0833333h;95%
With hydroxylamine hydrochloride; potassium carbonate In water; ethyl acetate at 0 - 20℃; for 16h;55%
4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

para-Chlorobenzyl alcohol
873-76-7

para-Chlorobenzyl alcohol

Conditions
ConditionsYield
With N-methylpyrrolidine zinc borohydride In tetrahydrofuran at 20℃; for 1.16667h;100%
With Zr(BH4)2Cl2(dabco)2 In tetrahydrofuran for 1.7h; Heating;98%
With sodium tetrahydroborate; lithium perchlorate In acetonitrile for 0.666667h;95%
3-amino-2-methyl-4-oxoquinazoline
1898-06-2

3-amino-2-methyl-4-oxoquinazoline

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

4-Chloro-N-(2-methyl-4-oxo-4H-quinazolin-3-yl)-benzamide
178919-58-9

4-Chloro-N-(2-methyl-4-oxo-4H-quinazolin-3-yl)-benzamide

Conditions
ConditionsYield
With pyridine In benzene for 2h; Heating;100%
In toluene Heating;
7-hydroxy-7,8,9,10-tetrahydrobenzopyrene
6272-55-5

7-hydroxy-7,8,9,10-tetrahydrobenzopyrene

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

7-(p-Chlorobenzoyloxy)-7,8,9,10-tetrahydrobenzo[a]pyrene

7-(p-Chlorobenzoyloxy)-7,8,9,10-tetrahydrobenzo[a]pyrene

Conditions
ConditionsYield
With pyridine; dmap In chloroform100%
N,O-dimethylhydroxylamine*hydrochloride
6638-79-5

N,O-dimethylhydroxylamine*hydrochloride

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

4-chloro-N-methoxy-N-methylbenzamide
122334-37-6

4-chloro-N-methoxy-N-methylbenzamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃;100%
Stage #1: N,O-dimethylhydroxylamine*hydrochloride With triethylamine In dichloromethane at 0℃; Inert atmosphere;
Stage #2: 4-chloro-benzoyl chloride In dichloromethane at 0 - 20℃; Inert atmosphere;
96%
With triethylamine In dichloromethane at 0 - 20℃;92%
4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

4-(3-hydroxyphenyl)piperidine
110878-71-2

4-(3-hydroxyphenyl)piperidine

1-(4-chlorobenzoyl)-4-(3-hydroxyphenyl)piperidine
325808-22-8

1-(4-chlorobenzoyl)-4-(3-hydroxyphenyl)piperidine

Conditions
ConditionsYield
With sodium hydroxide In isopropyl alcohol at 40 - 50℃; for 2h;100%
4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

t-butyl 5-benzyloxy-2-methyl indole acetate
346424-35-9

t-butyl 5-benzyloxy-2-methyl indole acetate

t-butyl 5-benzyloxy-1-(chlorobenzoyl)-2-methyl indole acetate

t-butyl 5-benzyloxy-1-(chlorobenzoyl)-2-methyl indole acetate

Conditions
ConditionsYield
Stage #1: t-butyl 5-benzyloxy-2-methyl indole acetate With potassium tert-butylate In tetrahydrofuran for 0.333333h;
Stage #2: 4-chloro-benzoyl chloride In tetrahydrofuran for 11h; Further stages.;
100%
4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

(1R/S,4R/S)-6S/R-(N,N-dimethylamino)-5S/R-phenylbicyclo<2.2.2>octan-2R/S-ol

(1R/S,4R/S)-6S/R-(N,N-dimethylamino)-5S/R-phenylbicyclo<2.2.2>octan-2R/S-ol

(1R/S,4R/S)-6R/S-(N,N-dimethylamino)-5R/S-phenylbicyclo[2.2.2]octan-2S/R-yl-4-chlorobenzoate

(1R/S,4R/S)-6R/S-(N,N-dimethylamino)-5R/S-phenylbicyclo[2.2.2]octan-2S/R-yl-4-chlorobenzoate

Conditions
ConditionsYield
With triethylamine; benzene100%
4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

(4-chlorophenyl)(2-methylaziridin-1-yl)methanone
21384-46-3

(4-chlorophenyl)(2-methylaziridin-1-yl)methanone

Conditions
ConditionsYield
With sodium hydroxide In diethyl ether at 0℃;100%
With sodium hydroxide In tetrahydrofuran89%
With sodium hydroxide In tetrahydrofuran89%
amino-4 hydroxy-2 toluene
2835-95-2

amino-4 hydroxy-2 toluene

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

4-chloro-benzoic acid 5-(4-chloro-benzoylamino)-2-methyl-phenyl ester
929290-81-3

4-chloro-benzoic acid 5-(4-chloro-benzoylamino)-2-methyl-phenyl ester

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 0 - 20℃; for 16h;100%
trifluorormethanesulfonic acid
1493-13-6

trifluorormethanesulfonic acid

4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

4-Chlorbenzoesaeure-trifluormethansulfonsaeure-anhydrid
36967-87-0

4-Chlorbenzoesaeure-trifluormethansulfonsaeure-anhydrid

Conditions
ConditionsYield
100%
4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

diisopropylamine
108-18-9

diisopropylamine

4-chloro-N,N-diisopropylbenzamide
79606-45-4

4-chloro-N,N-diisopropylbenzamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 6h;100%
With dmap; triethylamine In tetrahydrofuran; dichloromethane at 0 - 20℃; for 12h;89%
With triethylamine In dichloromethane at 20℃; Inert atmosphere;84%
4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

p-aminoiodobenzene
540-37-4

p-aminoiodobenzene

4-chloro-N-(4-iodo-phenyl)-benzamide
299954-64-6

4-chloro-N-(4-iodo-phenyl)-benzamide

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 20℃; for 4h;100%
With triethylamine In tetrahydrofuran at 20℃; for 4h;100%
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