N-benzyl-N-methylcarbamoyl chloride

Base Information

Chemical Name:N-benzyl-N-methylcarbamoyl chloride
CAS No.:32366-02-2
Molecular Formula:C9H10ClNO
Molecular Weight:183.637
Hs Code.:
European Community (EC) Number:694-490-9
Nikkaji Number:J525.739E

Synonyms:N-benzyl-N-methylcarbamoyl chloride;32366-02-2;benzyl(methyl)carbamic chloride;SCHEMBL3369887;Benzyl-methyl-carbamoyl chloride;N-benzyl-N-methylcarbamoylchloride;N-methyl-N-benzylcarbamoyl chloride;AKOS016359859;N-Methyl-N-benzylcarbamic acid chloride;Carbamic chloride, methyl(phenylmethyl)-;CS-0235076;EN300-152559

Suppliers and Price of N-benzyl-N-methylcarbamoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of N-benzyl-N-methylcarbamoyl chloride

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:183.0450916
Heavy Atom Count:12
Complexity:155

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(CC1=CC=CC=C1)C(=O)Cl

Technology Process of N-benzyl-N-methylcarbamoyl chloride

There total 2 articles about N-benzyl-N-methylcarbamoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.6%

: 32315-10-9
bis(trichloromethyl) carbonate

: 103-67-3
benzyl-methyl-amine

: 32366-02-2
benzyl(methyl)carbamic chloride

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h; Temperature;

Reference yield:

: 75-44-5
phosgene

: 13426-94-3
N-methylbenzylamine hydrochloride

: 32366-02-2
benzyl(methyl)carbamic chloride

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; toluene; at 0 ℃; for 2h;
DOI:10.1021/jm980131z

Reference yield: 94.0%

: 32366-02-2
benzyl(methyl)carbamic chloride

: 592526-88-0
2-Trimethylsilanyl-ethanesulfonic acid ((3aS,4R,6aR)-2-oxo-3,3a,4,6a-tetrahydro-2H-cyclopentaoxazol-4-yl)-amide

: 736993-83-2
(3aS,4R,6aR)-2-Oxo-4-(2-trimethylsilanyl-ethanesulfonylamino)-4,6a-dihydro-3aH-cyclopentaoxazole-3-carboxylic acid benzyl-methyl-amide

Guidance literature:: 2-Trimethylsilanyl-ethanesulfonic acid ((3aS,4R,6aR)-2-oxo-3,3a,4,6a-tetrahydro-2H-cyclopentaoxazol-4-yl)-amide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h;

benzyl(methyl)carbamic chloride; In tetrahydrofuran; hexane; for 4h; Heating;

With 1,4-diaza-bicyclo[2.2.2]octane; In tetrahydrofuran; hexane; for 18h; Heating;
DOI:10.1021/ol0490476