Methyl 2-iodo-6-nitrobenzoate

Base Information

Chemical Name:Methyl 2-iodo-6-nitrobenzoate
CAS No.:5471-78-3
Molecular Formula:C8H6INO4
Molecular Weight:307.044
Hs Code.:
NSC Number:28453
DSSTox Substance ID:DTXSID30970025

Synonyms:methyl 2-iodo-6-nitrobenzoate;5471-78-3;NSC28453;SCHEMBL16749890;DTXSID30970025;NSC-28453;2-iodo-6-nitrobenzoic acid methylester

Suppliers and Price of Methyl 2-iodo-6-nitrobenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Methyl 2-iodo-6-nitrobenzoate

Chemical Property:

Vapor Pressure:5.85E-06mmHg at 25°C
Boiling Point:379.4°C at 760 mmHg
Flash Point:148°C
Density:1.18g/cm³
XLogP3:1.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:306.93416
Heavy Atom Count:14
Complexity:240

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(=O)C1=C(C=CC=C1I)[N+](=O)[O-]

Technology Process of Methyl 2-iodo-6-nitrobenzoate

There total 3 articles about Methyl 2-iodo-6-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.8%

: 57113-89-0
2-amino-6-nitrobenzoic acid methylester

: 5471-78-3
2-iodo-6-nitrobenzoic acid methylester

Guidance literature:: 2-amino-6-nitrobenzoic acid methylester; With hydrogenchloride; sodium nitrite; In water; at 0 ℃; for 2h;

With potassium iodide; In water; at 60 ℃; for 1h; Heating;

Reference yield:

: 50573-74-5
6-nitroanthranilic acid

: 5471-78-3
2-iodo-6-nitrobenzoic acid methylester

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / N,N-dimethyl-formamide / 24 h / 20 °C

2.1: sodium nitrite; hydrogenchloride / water / 2 h / 0 °C

2.2: 1 h / 60 °C / Heating

With hydrogenchloride; triethylamine; sodium nitrite; In water; N,N-dimethyl-formamide;