bis[μ-(azido-κN:κN)][(μ-benzoato-κO:κO')]bis(1,4,7-triazacyclononane-κN(1),κN(4),κN(7))dinickel perchlorate hydrate

Base Information

Chemical Name:bis[μ-(azido-κN:κN)][(μ-benzoato-κO:κO')]bis(1,4,7-triazacyclononane-κN(1),κN(4),κN(7))dinickel perchlorate hydrate
CAS No.:633296-03-4
Molecular Formula:C₁₉H₃₅N₁₂Ni₂O₂*ClO₄*H₂O
Molecular Weight:698.412
Hs Code.:

Synonyms:

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Chemical Property of bis[μ-(azido-κN:κN)][(μ-benzoato-κO:κO')]bis(1,4,7-triazacyclononane-κN(1),κN(4),κN(7))dinickel perchlorate hydrate

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Technology Process of bis[μ-(azido-κN:κN)][(μ-benzoato-κO:κO')]bis(1,4,7-triazacyclononane-κN(1),κN(4),κN(7))dinickel perchlorate hydrate

There total 1 articles about bis[μ-(azido-κN:κN)][(μ-benzoato-κO:κO')]bis(1,4,7-triazacyclononane-κN(1),κN(4),κN(7))dinickel perchlorate hydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 532-32-1
sodium benzoate

: sodium azide

: nickel(II) perchlorate hexahydrate

: 4730-54-5
1,4,7-triazacyclononane

: 633296-03-4
bis[μ-(azido-κN:κN)][(μ-benzoato-κO:κO')]bis(1,4,7-triazacyclononane-κN(1),κN(4),κN(7))dinickel perchlorate hydrate

Guidance literature:: In methanol; water; addn. of a soln. of sodium benzoate in methanol to an aq. soln. of metalsalt, addn. of ligand and azide, heating at 50-70°C for 0.5 h; filtration, evapn. at room temp. over 1 wk; elem. anal.;
DOI:10.1002/hlca.200390197